`U.S. Patent No. 9,131,803
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`UNITED STATES PATENT AND TRADEMARK OFFICE
`__________________
`
`BEFORE THE PATENT TRIAL AND APPEAL BOARD
`__________________
`
`
`THE KINGSFORD PRODUCTS COMPANY, LLC
`Petitioner
`
`
`v.
`
`
`CREATIVE SPARK, LLC
`Patent Owner
`
`__________________
`
`
`Case IPR2016-01831
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`U.S. Patent No. 9,131,803
`Title: CHARCOAL BRIQUET AND PACKAGED CHARCOAL BRIQUET
`PRODUCT
`Issue Date: September 15, 2015
`
`__________________
`
`
`DECLARATION OF JAMES G. SPEIGHT, PH.D.
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`Exhibit 2021 Page 1
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`Creative Spark Exhibit 2021
`The Kingsford Products Co., LLC v. Creative Spark, LLC
`Case IPR2016-01831
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`
`
`Case IPR2016-01831
`U.S. Patent No. 9,131,803
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`TABLE OF CONTENTS
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`I.
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`INTRODUCTION ........................................................................................... 5
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`Page
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`II.
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`BASES FOR OPINIONS ................................................................................ 5
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`III. MATERIALS CONSIDERED ........................................................................ 6
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`IV. QUALIFICATIONS ........................................................................................ 7
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`A. Overview ............................................................................................... 8
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`B.
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`Experience With Briquetting, Carbonaceous Fuels, And Related
`Technologies ....................................................................................... 12
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`V.
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`LEGAL STANDARDS ................................................................................. 13
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`A. Anticipation ......................................................................................... 14
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`B.
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`Inherency ............................................................................................. 14
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`C. Obviousness ......................................................................................... 15
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`D. Written Description And Priority ........................................................ 18
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`VI. LEVEL OF ORDINARY SKILL IN THE ART ........................................... 18
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`VII. TECHNICAL BACKGROUND ................................................................... 19
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`A.
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`Ingredients Of Charcoal Briquets ........................................................ 19
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`1.
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`2.
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`3.
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`Base Fuels ................................................................................. 19
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`Binders ...................................................................................... 20
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`Ignition Aids ............................................................................. 21
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`Forming Briquets ................................................................................. 21
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`Physical Properties Of Charcoal Briquets ........................................... 23
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`B.
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`C.
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`Exhibit 2021 Page 2
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`Case IPR2016-01831
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`U.S. Patent No. 9,131,803
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`D.
`Combustion Of Charcoal Briquets ...................................................... 25
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`VIII. OPINIONS ..................................................................................................... 28
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`A. Opinions On Ground 1: Burke, Wulf, And Peters (Claims 1-32) ....... 28
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`1.
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`A Person Of Ordinary Skill In The Art Would Not Have
`Added Wulf’s Roller-Pressed Grooves To The Briquets
`Described In Burke And Peters................................................. 28
`
`i. Burke and Peters Discouraged The Use Of Grooves For
`Charcoal Briquets. ..................................................................... 29
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`ii. Roller Pressing Grooves Into Charcoal Briquets Would
`Lead To Briquets That Break Easily. ........................................ 36
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`2.
`
`Burke, Wulf, And Peters Do Not Meet The Time And
`Temperature Limitations Of The Claims. ................................. 45
`
`i. Burke .................................................................................... 49
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`ii. Wulf ..................................................................................... 58
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`iii. Peters .................................................................................. 58
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`iv. Other References ................................................................ 62
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`v. Summary Chart ................................................................... 67
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`3. Wulf Does Not Disclose Several Of The Claimed Groove
`Configurations. .......................................................................... 69
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`i. Relationship Between Groove Width And Depth ............... 70
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`ii. Grooves Symmetrical About A Horizontal Plane Through
`The Center Of The Briquet ....................................................... 72
`
`iii. Maximum Groove Depth No Deeper Than 25% Of
`Maximum Briquet Depth .......................................................... 75
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`4.
`
`There Was A Long-Felt Need For Charcoal Briquets
`Configured To Both Achieve A Cooking Temperature Of
`
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`Exhibit 2021 Page 3
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`Case IPR2016-01831
`U.S. Patent No. 9,131,803
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`1000ºF Within About 15 Minutes After Ignition And
`Sustain That Cooking Temperature For At Least 15
`Minutes Thereafter. ................................................................... 77
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`5.
`
`There Was Skepticism That Grooved Charcoal Briquets
`Could Provide Superior
`Ignition And Burning
`Characteristics. .......................................................................... 88
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`B. Opinions On Ground 3: Saunders II (Claims 1 and 9) ........................ 96
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`IX. APPENDIX A: THE CHALLENGED CLAIMS OF THE ’803
`PATENT ........................................................................................................ 99
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`X. APPENDIX B ..............................................................................................109
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`Exhibit 2021 Page 4
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`I.
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`INTRODUCTION
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`I, James G. Speight, a resident of Laramie, Wyoming over 18 years of age,
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`hereby declare as follows:
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`1.
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`I have personal knowledge of all of the matters about which I testify
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`in this declaration.
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`2.
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`Desmarais LLP retained me on behalf of Creative Spark, LLC to
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`provide my technical opinions and testimony about Claims 1-32 of U.S. Patent No.
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`9,131,803 (KNG1001, “the ’803 Patent”). I refer to those claims as the
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`“challenged claims.” The full text of the challenged claims appears in
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`Appendix A to my declaration.
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`3.
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`I am being compensated for my work in this proceeding at my usual
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`rate of $150/hour and receiving reimbursement for expenses incurred in the course
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`of my work. My compensation is not contingent in any way on either the opinions
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`I have reached or the outcome of this case.
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`II. BASES FOR OPINIONS
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`4.
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`I have reviewed, analyzed, and relied upon the documents and other
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`materials listed below in Section III in light of my specialized knowledge provided
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`by my education, training, research, and experience, as summarized in Section IV
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`and described in detail in my CV, which is provided as Appendix B. My analysis
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`of those materials, combined with the specialized knowledge that I have obtained
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`Exhibit 2021 Page 5
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`over the course of my education and career, form the bases for my opinions in this
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`declaration.
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`III. MATERIALS CONSIDERED
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`5.
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`I have reviewed, analyzed, and relied upon the parties’ papers and
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`exhibits in this proceeding, including the ’803 Patent (KNG1001) and its file
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`history (KNG1010); the Petition and its accompanying exhibits, including Wulf
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`(KNG1004), Peters (KNG1006), Burke (KNG1007), Saunders II (KNG1009); Dr.
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`Smith’s declaration (KNG1002) and deposition transcript; Creative Spark’s
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`preliminary response; and the Board’s institution decision. I have also reviewed,
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`analyzed, and relied upon each of the exhibits cited in this declaration, including
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`the following:
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`-
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`-
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`-
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`-
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`S.R. Richards, Physical Testing of Fuel Briquettes, 25 FUEL
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`PROCESSING TECHNOLOGY 89 (1990) (Ex. 2011, “Richards”);
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`A.N.E. Rahman, Influence of Size and Shape on the Strength of
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`Briquettes, 23 FUEL PROCESSING TECHNOLOGY 185 (1989) (Ex. 2012,
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`“Rahman”);
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`J. Mills, Binders for Coal Briquets, United States Geological Survey
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`Bulletin 343 (1908) (Ex. 2013, “Mills”);
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`J.S.S. BRAME, FUEL: SOLID LIQUID AND GASEOUS (1914) (Ex. 2014,
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`“Brame”);
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`Exhibit 2021 Page 6
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`-
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`-
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`JOHN PERCY, METALLURGY: THE ART OF EXTRACTING METALS FROM
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`THEIR ORES (1875) (Ex. 2015, “Percy”);
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`M.T. Taghizadeh and Reza Abdollahi, A Kinetics Study on the
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`Thermal Degradation of Starch/Poly (Vinyl Alcohol) Blend, 3 CHEM.
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`& MATS. ENG’G 73 (2015) (Ex. 2016, “Taghizadeh”);
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`-
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`Robert Shanks & Ing Kong, Thermoplastic Starch, in THERMOPLASTIC
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`ELASTOMERS (Prof. Adel El-Sonbati, ed.) (2012) (Ex. 2017,
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`“Shanks”);
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`-
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`-
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`U.S. Patent No. 3,328,187 to Mennen (1967) (Ex. 2018, “Mennen”);
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`R.J. Hamor et al., Kinetics of Combustion of a Pulverized Brown Coal
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`Char Between 630 and 2200 K, 21 COMBUSTION & FLAME 153 (1973)
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`(Ex. 2019, “Hamor”); and
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`-
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`Excerpts from “Industrial charcoal making,” FAO Forestry Paper 63,
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`Food and Agriculture Organization of the United Nations (1985),
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`available
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`at
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`http://www.fao.org/docrep/x5555e/x5555e00.htm.
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`(Ex. 2020).
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`IV. QUALIFICATIONS
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`6.
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`I have summarized my education and experience below. In addition
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`to the summary I have provided here, I describe my education and experience in
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`greater detail in my CV, attached as Appendix B.
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`Exhibit 2021 Page 7
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`A. Overview
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`7.
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`I have a Bachelor of Science degree (Honors) in Chemistry and a
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`Ph.D. in Organic Chemistry from the University of Manchester, Manchester,
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`England, a Doctor of Science (Honoris Causa) in Geological Sciences from the
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`Scientific Research Geological Exploration Institute (VNIGRI) in St. Petersburg,
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`Russia, and a Ph.D. in Petroleum Engineering from Dubna International
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`University, Moscow District, Russia. I am a Chartered Chemist of the Royal
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`Society of Chemistry (UK). I am also a Fellow of the Royal Society of Chemistry
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`(UK), a Fellow of the Chemical Institute of Canada, and a Member of the
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`American Chemical Society.
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`8.
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`From 1965 to 1967, I was employed as an Imperial Chemical
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`Industries Research Fellow in Chemistry at the University of Manchester.
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`9.
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`From 1967 to 1980, I was employed by the Alberta Research Council
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`as a Research Officer and Manager of the Coal Technology Information Center.
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`Additionally, from 1976-1980, I was appointed as a Visiting Lecturer in petroleum
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`science at the University of Alberta in Edmonton, Alberta, and in 1978, was a
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`Visiting Lecturer in petroleum science at the University of Mosul in Iraq. When in
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`Mosul, I taught petroleum technology (production and refining) and co-supervised
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`one Master of Science student and two Ph.D. students.
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`Exhibit 2021 Page 8
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`10. From 1980-1984, I was a Research Associate in Exxon Research and
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`Engineering in New Jersey where I worked on the recovery, properties, and
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`refining of Cold Lake heavy oil, including the use of carbonaceous residua as
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`sources of fuel.
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`11. From 1984-1989, I was the Chief Scientific Officer (and Deputy
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`Managing Director) of the Western Research Institute in Laramie, Wyoming.
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`Western Research Institute is a multimillion-dollar research organization which
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`provides a variety of research and development services, including services related
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`to crude oil recovery, refining, and product properties. In this position, I managed
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`and directed the scientific and engineering research efforts of the Institute. From
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`1990-1998, I was the Chief Executive Officer of the Western Research Institute.
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`The duties included the general management and administrative duties as well as
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`oversight of all the scientific and engineering activities of the Western Research
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`Institute including continued technical oversight of all contracts.
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`12. Additionally, from 1984-1998 I was an Adjunct Professor of
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`Chemistry at the University of Wyoming, and from 1991-1998 was also an
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`Adjunct Professor of Chemical Engineering at the University of Wyoming.
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`13. From 1993-2005, I was also an Adjunct Professor of Chemical and
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`Fuels Engineering at the University of Utah.
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`Exhibit 2021 Page 9
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`14. Since 1998, I have been Secretary-Treasurer of CD&W Inc., a
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`Laramie-based contract-funded company that was founded in Laramie, Wyoming
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`which offers consulting in the areas of petroleum recovery and petroleum refining
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`as well as other technical services to national and international clients.
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`15. From 2005-2009, I was a Visiting Professor at the University of
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`Trinidad and Tobago, Point Lisas, Trinidad where I taught classes in petroleum
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`technology as well as the properties and refining of various local heavy oils and tar
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`sand bitumen and the conversion of the high-boiling portions of these feedstocks to
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`carbonaceous fuels.
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`16.
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`I currently serve as the Editor of three peer-reviewed scientific
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`journals: (i) Petroleum Science and Technology – Founding Editor and Editor since
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`1983, as well as (ii) Energy Sources Part A: Recovery, Utilization, and
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`Environmental Effects – Editor since 1993, and (iii) Energy Sources Part B:
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`Economics, Planning, and Policy – Founding Editor and Editor since 2006. The
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`three Journals are published by Taylor & Francis (London, United Kingdom, and
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`Philadelphia, USA).
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`17.
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`I have been the author, co-author, or editor of more than seventy
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`books and bibliographies as well as four databases related to fossil fuel processing
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`and
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`the associated environmental
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`issues,
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`including
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`the recently-published
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`Chemistry and Technology of Coal, 3rd Edition (2013); Chemistry and Technology
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`Exhibit 2021 Page 10
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`of Petroleum, 5th Edition (2014); and Handbook of Petroleum Refining (2017). In
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`addition, I have authored more than 400 publications, reports, and presentations,
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`many of which relate to petroleum and coal technology, and have taught more than
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`80 courses. A full list of the books, publications, and courses taught is presented in
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`Appendix B.
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`18. Throughout my career, I have earned various awards, including the
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`following:
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`-
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`Appointed as the Scientific Representative for the State of Wyoming
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`to the National Governor’s Association Task Force on State Applied
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`-
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`-
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`-
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`Research from 1986-87, and again from 1987-1993.
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`Diploma of Honor from the National Petroleum Engineering Society
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`for Outstanding Contributions to the Petroleum Industry in 1995.
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`Gold Medal from the Russian Academy of Sciences for Outstanding
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`Work in Petroleum Science in 1996.
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`The Einstein Medal of the Russian Academy of Sciences in
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`recognition of Outstanding Contributions and Service in the field of
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`Geologic Sciences, 2001.
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`-
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`Methanex Distinguished Professor, University of Trinidad and
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`Tobago in recognition of Excellence in Research, 2006.
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`Exhibit 2021 Page 11
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`Gold Medal – Giants of Science and Engineering, Russian Academy
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`of Sciences in recognition of Continued Excellence in Science and
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`Engineering, 2006.
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`B.
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`Experience With Briquetting, Carbonaceous Fuels, And Related
`Technologies
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`19.
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`In addition to the experience I have described above, my experience
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`includes production and properties of carbonaceous briquets from coal, tar sand
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`bitumen, heavy oil residua, and blends thereof. This work commenced in 1967
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`while I was in Alberta and continued while I was at Exxon as well as during my
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`time at the Western Research Institute.
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`20. Further, while working as a visiting professor at the University of
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`Mosul in Iraq in 1978, I also studied the carbonization of Qayarah heavy oil and its
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`potential for use as a carbonaceous fuel in the form of briquets. During this time, I
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`wrote several reports on the chemical and physical properties of briquets produced
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`from Qayarah heavy oil.
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`21. Since leaving the Western Research Institute in 1998, I have worked
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`as a consultant on projects related to carbonization of coal, tar sand bitumen, and
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`heavy oil residua as well as the production and properties of briquets of various
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`blends of these materials.
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`Exhibit 2021 Page 12
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`22. Subsequently, during my appointment as Visiting Professor at the
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`University of Trinidad and Tobago (2005-2009), I worked with the Trinidad Lake
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`bitumen, its pelletization and carbonization for sale as a fuel.
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`V. LEGAL STANDARDS
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`23. Creative Spark’s attorneys have explained to me the legal standards
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`that apply in this case. My understanding of those standards is described below. I
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`am not an attorney, and I do not have formal training in the law regarding patents.
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`I have used my understanding of the following legal principles set forth in this
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`section in reaching my opinions.
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`24.
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`I understand that this proceeding is before the Patent Trial and Appeal
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`Board. I understand that Kingsford has the burden of proving that the challenged
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`claims are invalid by a preponderance of the evidence.
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`25.
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`I understand that because this is a Patent Trial and Appeal Board
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`proceeding involving an unexpired patent, the patent’s claims are to be given their
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`broadest reasonable interpretation in light of the specification and prosecution
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`history of the patent. I understand that claim construction at the Patent Trial and
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`Appeal Board works somewhat differently than it does in a federal district court, in
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`which claims are construed according to their ordinary and customary meaning in
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`light of the specification and file history of the patent in which those claims appear.
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`Exhibit 2021 Page 13
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`26.
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`I understand that it is necessary to analyze the claims of a patent and
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`the prior art from the perspective of a person of ordinary skill in the art at the time
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`of the invention claimed in the patent.
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`27.
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`I understand that a claim that depends from another claim incorporates
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`all of the limitations from that claim. If a claim is not anticipated or obvious, then
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`a claim that depends from that claim is not anticipated or obvious, either.
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`A. Anticipation
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`28.
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`I understand that to anticipate a claim of a patent, a prior art reference
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`must disclose, either expressly or inherently, all limitations of a claim as those
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`limitations are arranged in the claim.
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`29.
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`I further understand that for a reference to be considered anticipating
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`it must disclose the relevant technology in a manner such that a person of ordinary
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`skill in the relevant art would be able to carry out or utilize the technology that the
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`reference describes without having to undertake undue experimentation.
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`B.
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`Inherency
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`30.
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`I understand that a limitation is disclosed inherently in a reference
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`only if it is necessarily present in the process or product described in the prior art
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`reference.
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`Exhibit 2021 Page 14
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`31.
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`I understand that probabilities or possibilities are insufficient to show
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`that a prior art reference inherently discloses something beyond what it discloses
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`explicitly.
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`C. Obviousness
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`32.
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`I understand that a claim is unpatentable as obvious if the differences
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`between the claim and the prior art are such that the subject matter as a whole
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`would have been obvious at the time the invention was made to a person having
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`ordinary skill in the art to which the subject matter pertains at the time of the
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`invention.
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`33.
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`I understand that obviousness is a question of law based on underlying
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`factual issues. Those factual issues are: (1) the scope and content of the prior art;
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`(2) differences between the prior art and the claimed invention as a whole; (3) the
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`level of ordinary skill in the art at the time the invention was made; and (4)
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`objective indicia of non-obviousness.
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`34.
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`I understand that an obviousness case based on modifying or
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`combining one or more prior art references requires the petitioner to show that a
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`person of ordinary skill in the art would have had a reason to modify or combine
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`those prior art references to achieve the claimed invention.
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`35.
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`I understand that an obviousness case based on modifying or
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`combining one or more prior art references also requires the petitioner to show that
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`Exhibit 2021 Page 15
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`a person of ordinary skill in the art would have had a reasonable expectation of
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`successfully achieving the claimed invention.
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`36.
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`I understand that example reasons to combine or modify prior art
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`references that may support a conclusion of obviousness include combining prior
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`art elements according to known methods to yield predictable results; simple
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`substitution of one known element for another to obtain predictable results; use of
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`a known technique to improve similar techniques; combining elements in a way
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`that would be “obvious to try” where there exists a finite number of identified,
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`predictable solutions and a reasonable expectation of success; design incentives or
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`market forces that would prompt variations of known work if those variations were
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`predictable to a person of ordinary skill in the art; a teaching, suggestion, or
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`motivation in the prior art to combine or modify prior art references to arrive at the
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`claimed subject matter; and optimization of a recognized result-effective variable
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`by a person of ordinary skill in the art if that optimization would be routine.
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`37.
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`I understand that there are also reasons that would prevent a person of
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`ordinary skill in the art from modifying or combining prior art references.
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`Examples of prior art references that a person of ordinary skill in the art would not
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`combine or modify to achieve the claimed invention include prior art references
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`that teach away from one another; prior art references that teach away from the
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`claimed invention; prior art references whose combination or modification would
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`Exhibit 2021 Page 16
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`change the principle of operation of either prior art reference; prior art references
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`whose combination or modification would render them inoperable or unsuitable for
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`their intended purpose; and prior art references whose combination or modification
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`would destroy a key objective of that prior art reference.
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`38.
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`I understand that in determining whether a person of ordinary skill in
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`the art would combine or modify prior art references, the entire contents of each
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`prior art reference must be considered, including parts of those references that
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`would suggest against the proposed combination or modification.
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`39.
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`I understand that objective indications of non-obviousness or
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`“secondary considerations,” if established, can weigh in favor of a finding of
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`non-obviousness. A nonexhaustive list of secondary considerations includes: long-
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`felt need, failure of others, and skepticism of experts.
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`40.
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`I understand that “secondary considerations” must be related or
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`connected to the language of the claims, and that this relationship is sometimes
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`called “nexus.” Nexus may be found if the secondary considerations relate to an
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`individual novel, non-obvious feature or to a novel, non-obvious combination of
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`features in a claim.
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`Exhibit 2021 Page 17
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`D. Written Description And Priority
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`41.
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`I understand that whether a claim in a child application can claim
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`priority to a parent application requires considering whether the claim has “written
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`description” support in the parent application.
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`42.
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`I understand that written description turns on whether a person of
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`ordinary skill in the art would recognize from the disclosure of the parent
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`application that the applicant had possession of the subject matter of the claim in
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`the child application as of the filing date of the parent application.
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`43.
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`I understand that Creative Spark has alleged that all of the challenged
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`claims are entitled to a priority date at least as early as (or no later than) June 1,
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`2004, the filing date of the application that published as Saunders II. (KNG1009,
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`at Cover.) I understand that Petitioner alleges that Claims 1-9 and 29 are not
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`entitled to a priority date any earlier than the filing date of the ’803 Patent on April
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`29, 2011.
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`VI. LEVEL OF ORDINARY SKILL IN THE ART
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`44. For my analysis, I have assumed the level of ordinary skill in the art
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`provided by Petitioner and Dr. Smith, which is “at least a B.S. degree in
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`mechanical or chemical engineering with at least one year of relevant industry
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`experience in combustion, briquetting, solid fuels, fire causation, or a related
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`field.” (Petition at 3-4; KNG1002 ¶ 21.) I have also assumed that that level of
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`Exhibit 2021 Page 18
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`ordinary skill in the art applies in 2002, 2004, and 2011, as Petitioner and Dr.
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`Smith posited. (Petition at 4; KNG1002 ¶ 22.)
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`45.
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`I had sufficient education and experience to qualify as a person of
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`ordinary skill in the art as of 2002, 2004, and 2011, as described above in
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`Section IV.
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`VII. TECHNICAL BACKGROUND
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`A.
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`Ingredients Of Charcoal Briquets
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`1.
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`Base Fuels
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`46. The ’803 Patent describes charcoal briquets as being “conventionally
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`fabricated from base fuels such as charred wood, coal, charred agricultural waste,
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`and similar products.” (’803 Patent at 1:48-50.)
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`47. Those charred materials are typically produced by a slow pyrolysis
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`process in which the wood or other materials are heated in the absence of oxygen
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`to carbonize them. (KNG1007, at 5:33-41; Ex. 2015, at 374.) The carbonization
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`process produces charcoal in various sizes, from lump charcoal to charcoal fines.
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`(Ex. 2020, at 18.)
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`48. The charcoal fines are then dried and screened by size. Charcoal fines
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`smaller than 2 to 4 mm in size are generally rejected: those fines typically come
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`from bark, twigs, and leaves, and have a higher ash content than normal wood
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`charcoal. (Ex. 2020, at 18.) Larger charcoal fines are generally acceptable for
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`Exhibit 2021 Page 19
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`briquetting. Those charcoal fines that are sufficiently large for use in briquetting
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`are broken down into charcoal powder, typically by hammer-milling. (Ex. 2020, at
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`18.)
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`2.
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`Binders
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`49. Because charcoal lacks plasticity, it often requires the addition of a
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`binder to enable a briquet to be formed. (Ex. 2020, at 18.) The binder should
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`preferably be combustible, though a non-combustible binder effective at low
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`concentrations can be suitable. (Id.)
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`50. Starch is a common binder, and the ’803 Patent identifies vegetable
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`starch as an example of a conventional binder. (’803 Patent at 1:50-52.) Starch for
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`use in briquetting is commonly formed into a paste to be mixed with the charcoal
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`powder. (KNG1007, at 5:47-50; Ex. 2013, at 37.)
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`51. Highly plastic clays can be suitable for use as the binder, providing
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`not more than about 15% w/w (weight per weight) is used. (Ex. 2020, at 18.)
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`However, including clay as a binder lowers the calorific value of the briquet (the
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`amount of heat it can produce during combustion) and makes the briquet ignite less
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`readily. (Ex. 2013, at 10.) Further, the use of an inorganic substance such as clay
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`as a binder (or as a constituent of the binder), tends to make the briquet ignite less
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`readily and increases the amount of ash produced, which can hinder the
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`combustion of the briquet. (Id. at 10, 24-25.)
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`52.
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`It is also worth noting that during ignition and burning, binders break
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`down from the heat produced by the burning charcoal briquet. For example, starch
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`binder begins to break down as low as 572 degrees Fahrenheit (300 degrees
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`Celsius) and substantially disintegrates during ignition and combustion. (Ex. 2016,
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`at 3; Ex. 2017, at 12; Ex. 2018, at 3:18-19, 3:41-44.)
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`3.
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`Ignition Aids
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`53. Because charcoal does not always ignite easily, charcoal briquets may
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`incorporate ignition aids, which are materials that ignite more quickly than the base
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`fuel in the briquet. (’803 Patent at 1:52-54.) Wax and sodium nitrate are common
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`ignition aids. (KNG1007, at 5:43-46; Ex. 2020, at 19.)
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`B.
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`Forming Briquets
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`54. To form a briquet, the charcoal powder obtained from the charcoal
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`fines is combined with any binders (such as starch) and ignition aids to form a
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`mixture. That mixture is then formed into a briquet by rolling, extruding, or
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`pressing. (KNG1007, at 5:42-51.)
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`55. Roller pressing has been used to create ungrooved charcoal briquets.
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`Roller pressing generally involves two adjacent rollers, between which charcoal
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`mixture for pressing is deposited and pressed into briquets. An example of roller
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`pressing is shown in Figure 1 of U.S. Patent No. 5,049,333 to Wolfe et al. (Ex.
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`2005, “the ’333 Patent.”)
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`56. As the ’333 Patent describes, “[i]n roll presses, particulate material is
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`compacted by squeezing as it is carried into the gap or pinch area 33 between two
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`tangentially interacting press rolls 8, 9, rotating at equal speed. . . . In other prior
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`art briquetting equipment, pillow shapes are formed by corresponding (matching)
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`indentations in each of the rolls.” (Ex. 2005, at 3:59-68.)
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`57. The formed briquet is then dried so that the binder can set. When
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`starch paste is used as a binder, the starch binds the briquet through the loss of
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`water. (KNG1007, at 5:56-6:7.)
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`C.
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`Physical Properties Of Charcoal Briquets
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`58. Richards describes that two important physical properties of charcoal
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`briquets are their compressive strength and their impact resistance. (Ex. 2011, at
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`2-3.)
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`59.
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`“Compressive strength is the maximum crushing load a briquette can
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`withstand before cracking or breaking.” (Ex. 2011, at 3.) For charcoal briquets,
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`compressive strength can be tested by placing a briquet between two horizontally-
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`oriented parallel plates, then applying a constantly increasing load until the briquet
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`cracks or breaks. (Id. at 3-4.)
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`60. According to Rahman, a briquet’s compressive strength varies
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`depending on the nature of the load applied to the briquet. (Ex. 2012, at 10-11.)
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`For example, “[t]he surface compression strength of cylindrical briquets is about
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`10 times the line and point compression strengths” of such briquets. (Id. at 10.) As
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`another example, a pillow-shaped briquet has a point compressive strength
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`approximately one-fifth of the surface compressive strength of a cylindrical briquet
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`of similar composition. (Id. at 10-11.)
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`61.
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`It is important for charcoal briquets to have enough compressive
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`strength to withstand the crushing loads that they regularly experience: “[f]uel
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`briquettes need to be able to withstand the crushing loads they receive in handling,
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`transport, storage, and firing.” (Ex. 2011, at 2.)
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`62.
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`Impact resistance refers to the ability of a briquet to withstand impacts
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`without breaking or cracking. (Ex. 2011, at 5.) “Impact resistance testing is
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`considered to be the best general diagnostic of briquette strength.” (Id.)
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`63. A briquet’s impact resistance can be measured using a drop test, in
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`which a briquet is dropped from a predetermined height, such as two meters. (Ex.
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`2011, at 5.) If the briquet does not break on the first drop, it is dropped again and
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`again until it does break, at which time the number of pieces that the briquet breaks
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`into are counted. (Id.) Impact resistance can be quantified using an impact
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`resistance index (IRI), as defined in the following equation from Richards:
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`64.
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`Impact resistance is important for charcoal briquets because charcoal
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`briquets sustain many impacts, including being dropped off trucks onto the ground
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`(Ex. 2011, at 2) and, more commonly, being poured from a bag into a metal grill or
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`barbecue pit during use in cooking. (’803 Patent, at 1:61-63, 2:2-5.)
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`D. Combustion Of Charcoal Briquets
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`65. Charcoal briquets are commonly employed as fuel for use in cooking,
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`such as in grills, grates, and pits. (’803 Patent at 1:22-24, 1:61-63.)
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`66. The efficiency of a charcoal briquet as a source of heat energy for
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`cooking is dependent upon two factors: (i) the ignition time and (ii) the
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`sustainability of the burn, which is subject to the burning rate (also called burn rate
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`or combustion rate) of the briquets. It is desirable for a briquet to have a short
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`ignition time and a long, sustained burn after completion of the ignition phase