Filed on behalf of Baker Hughes, a GE Company, LLC
`
`By: Herbert D. Hart III
`
`George F. Wheeler
`
`Aaron F. Barkoff
`
`Peter J. Lish
`McAndrews, Held & Malloy, Ltd.
`500 W. Madison St., 34th Floor
`Chicago, IL 60661
`Tel: 312-775-8000
`Fax: 312-775-8100
`E-mail: hhart@mcandrews-ip.com
`
`
`
`
`UNITED STATES PATENT AND TRADEMARK OFFICE
`_____________
`
`BEFORE THE PATENT TRIAL AND APPEAL BOARD
`_____________
`
`BAKER HUGHES, a GE COMPANY, LLC
`(f/k/a BAKER HUGHES INCORPORATED),
`Petitioner,
`
`v.
`
`LIQUIDPOWER SPECIALTY PRODUCTS INC.
`(f/k/a LUBRIZOL SPECIALTY PRODUCTS, INC.),
`Patent Owner.
`_____________
`
`Case IPR2016-01901
`Patent No. 8,450,249 B2
`_____________
`
`PETITIONER’S UPDATED EXHIBIT LIST
`
`
`
`By: Herbert D. Hart III
`
`George F. Wheeler
`
`Aaron F. Barkoff
`
`Peter J. Lish
`McAndrews, Held & Malloy, Ltd.
`500 W. Madison St., 34th Floor
`Chicago, IL 60661
`Tel: 312-775-8000
`Fax: 312-775-8100
`E-mail: hhart@mcandrews-ip.com
`
`
`
`
`UNITED STATES PATENT AND TRADEMARK OFFICE
`_____________
`
`BEFORE THE PATENT TRIAL AND APPEAL BOARD
`_____________
`
`BAKER HUGHES, a GE COMPANY, LLC
`(f/k/a BAKER HUGHES INCORPORATED),
`Petitioner,
`
`v.
`
`LIQUIDPOWER SPECIALTY PRODUCTS INC.
`(f/k/a LUBRIZOL SPECIALTY PRODUCTS, INC.),
`Patent Owner.
`_____________
`
`Case IPR2016-01901
`Patent No. 8,450,249 B2
`_____________
`
`PETITIONER’S UPDATED EXHIBIT LIST
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`
`EXHIBIT
`1001
`1002
`1003
`1004
`
`1005
`
`1006
`
`1007
`
`1008
`
`1009
`
`1010
`
`1011
`
`1012
`
`1013
`
`1014
`
`
`DESCRIPTION
`U.S. Patent No. 8,022,118 B2 (“the 118 patent”)
`U.S. Patent No. 8,426,498 B2 (“the 498 patent”)
`U.S. Patent No. 8,450,249 B2 (“the 249 patent”)
`U.S. Patent No. 8,450,250 B2 (“the 250 patent”)
`Holtmyer, Marlin D. and Chatterji, Jiten, “Study of Oil Soluble
`Polymers as Drag Reducers,” Polymer Engineering and Science,
`vol. 20, no. 7, 1980 (“the Holtmyer Publication”).
`U.S. Patent No. 3,758,406, “Methods and Compositions for
`Reducing Frictional Pressure Loss in the Flow of Hydrocarbon
`Liquids,” granted 9/11/1973 (“the Holtmyer Patent”)
`European Patent Application No. EP 0,882,739 A2, High molecular
`weight polymer and producing method the same and drag reducer,
`published 12/9/1998 (“Inaoka”)
`Carnahan, Norman F., “Precipitation of Asphaltenes in Heavy Oil
`and Tar Sands,” in Asphaltenes and Asphalts, 2, Developments in
`Petroleum Science 40B, Elsevier Science B.V., 2000 (“Carnahan”)
`Strausz, O.P. and Lown, E.M., The Chemistry of Alberta Oil Sands,
`Bitumens and Heavy Oils, Alberta Energy Research Institute,
`Calgary, 2003 (“Strausz”)
`Curriculum Vitae of Thomas H. Epps III, Ph.D.
`Brandrup et al., Polymer Handbook, 4th ed., John Wiley & Sons,
`Inc., 1999 (“Brandrup”)
`Young & Lovell, Introduction to Polymers, 2nd ed., CRC Press,
`1991 (“Young & Lovell”)
`Odian, George, Principles of Polymerization, 4th ed., John Wiley &
`Sons, Inc., 2004 (“Odian”)
`Zakin, J.L. and Hunston, D.L., “Effect of Polymer Molecular
`Variables on Drag Reduction,” J. Macromol. Sci.-Phys., B18(4),
`795-814 (1980)
`
`2
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`EXHIBIT
`
`DESCRIPTION
`Mowla, D. and Naderi, A., “Experimental study of drag reduction
`by a polymeric additive in slug two-phase flow of crude oil and air
`in horizontal pipes,” Chemical Engineering Science 61, 1549-1554,
`available online as of November 4, 2005
`Burger et al., “Studies of Drag Reduction Conducted over a Broad
`Range of Pipeline Conditions when Flowing Prudhoe Bay Crude
`Oil,” Journal of Rheology, 24(5), 603-626 (1980)
`Buckley, J.S., et al., “Asphaltene Precipitation And Solvent
`Properties of Crude Oils,” Petroleum Science and Technology, vol.
`16, no. 3-4, 1998
`Ferguson, K.R., et al., “Microbial Pilot Test for the Control of
`Paraffin and Asphaltenes at Prudhoe Bay,” Society of Petroleum
`Engineers, Inc., 1996
`U.S. Pat. Appl. No. 11/615,539, Preliminary Amendment, Mar. 10,
`2008
`U.S. Pat. Appl. No. 11/615,539, Request for Reconsideration to
`Office Action, Jun. 24, 2009
`U.S. Pat. Appl. No. 11/615,539, Request for Reconsideration to
`Office Action, Apr. 8, 2010
`U.S. Pat. Appl. No. 11/615,539, Response to Final Office Action,
`Aug. 27, 2010
`U.S. Pat. Appl. No. 11/615,539, Affidavit Under 37 CFR 1.132,
`signed by Ray L. Johnston, Aug. 13, 2010
`U.S. Pat. Appl. No. 11/615,539, Office Action, Nov. 18, 2010
`U.S. Pat. Appl. No. 11/615,539, Response to Office Action, Apr. 8,
`2011
`U.S. Pat. Appl. No. 11/615,539, Notice of Allowance and Fees Due,
`May 11, 2011
`
`1015
`
`1016
`
`1017
`
`1018
`
`1019
`
`1020
`
`1021
`
`1022
`
`1023
`
`1024
`
`1025
`
`1026
`
`3
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`EXHIBIT
`
`1027
`
`1029
`
`1030
`
`1028
`
`DESCRIPTION
`Martinez-Palou, R. et al., “Transportation of Heavy and Extra-
`Heavy Crude Oil by Pipeline: A Review,” J. Pet. Sci. Eng. 75:274-
`82, 2011
`Conoco CDR® 102 Flow Improver, filed in U.S. Pat. Appl. No.
`381,232, issued as U.S. Pat. No. 4,983,186, Jan. 8, 1991
`ConocoPhillips LPTM 300 Product Datasheet, accessed at
`https://web.archive.org/web/20040604182725/http://liquidpower.co
`m/ProductSolution/ProductSolution.asp
`ConocoPhillips LPTM 400 Product Datasheet, accessed at
`https://web.archive.org/web/20040604182725/http://liquidpower.co
`m/ProductSolution/ProductSolution.asp
`1031-33 Reserved
`1034
`U.S. Pat. Appl. No. 13/208,063, Office Action, Dec. 3, 2012
`U.S. Pat. Appl. No. 13/208,063, Amendment and Response to
`Office Action, Jan. 16, 2013
`U.S. Pat. Appl. No. 13/208,063, Notice of Allowance and Fees Due,
`Dec. 13, 2013
`1037-38 Reserved
`Transcript of Deposition of Brian Dunn, Ph.D., (excerpt), Lubrizol
`Specialty Prods., Inc. v. Baker Hughes Inc., No. 4:15-cv-02915
`(S.D. Tex.), Feb. 9, 2016
`Horn, A.F. et al., “High Viscosity Crude Drag Reduction,” Pipeline
`& Gas Journal, pages 22-25, June 1986.
`Declaration of Professor Thomas H. Epps, III
`1041
` 1042–60 Reserved
`1061 Morrison, Robert Thornton and Boyd, Robert Neilson, “Organic
`Chemistry,” Second Edition, 1966, page 109
`
`1035
`
`1036
`
`1039
`
`1040
`
`4
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`EXHIBIT
`
`1062
`
`DESCRIPTION
`Meyer, Richard and Attanasi, Emil, “Heavy Oil and Natural
`Bitumen—Strategic Petroleum Resources,” U.S. Geological Survey
`Fact Sheet 70-03 August 2003 – Online Version 1.0.
`PowerPoint, BH013805-15 (redacted version of Ex. 2082)
`1063
`PowerPoint, BH014546, BH014554 (redacted version of Ex. 2083)
`1064
`1065-67 Reserved
`1068
`Transcript of Conference Call, August 29, 2017
`1069
`Amended Protective Order
`1070
`List (Confidential)
`1070
`List (Redacted)
`1071
`E-mail of August 21, 2017
`Transcript from August 25, 2017 cross-examination of Brian Dunn,
`Ph.D. (Confidential)
`ConocoPhillips ExtremePower™ brochure titled “Heavy Oil Market
`Study”
`Technical Services Report, LSPI_DRA_0057359-68 (Confidential)
`Technical Services Report, LSPI_DRA_0057402-30 (Confidential)
`Technical Services Report, LSPI_DRA_0057431-36 (Confidential)
`Transcript from the deposition of Yung Nam Lee,
`Ph.D., Director of Engineering and Technical Services
`for Patent Owner, in Civil Action No. 4:15-cv-02915,
`March 16, 2017 – pages 103, 120, 126 (Confidential)
`Technical Service Report, LSPI_DRA_0060152-63 (Confidential)
`Srinivasan & Watkinson, Fouling of Some Canadian Crude Oils,
`Heat Exchanger Fouling and Cleaning: Fundamentals and
`Applications, Engineering Conferences International, 2003
`
`1074
`1075
`1076
`
`1072
`
`1073
`
`1077
`
`1078
`
`1079
`
`5
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`EXHIBIT
`
`DESCRIPTION
`ExxonMobil assay sheet for Cold Lake crude oil, available at
`http://corporate.exxonmobil.com/en/company/worldwide-
`operations/crude-oils/cold-lake-blend
`Ray Johnston et al., New Heavy Crude Oil Flow Improver Increases
`Delivery – Application Scenarios, 5th NCUT Upgrading and
`Refining Conference 2009
`Cortes et al., Biomarkers and compound-specific stable carbon
`isotopes of n-alkanes in crude oils from Eastern Llanos Basin,
`Colombia, Journal of South American Earth Sciences, vol. 29,
`pages 198-213 (2010)
`Email, LSPI_DRA_0036927-28 (Confidential)
`Email, LSPI_DRA_0060263 (Confidential)
`Email, LSPI_DRA_0062832-33 (Confidential)
`Email, LSPI_DRA_0036378 (Confidential)
`Email, LSPI_DRA_0036379 (Confidential)
`Martin et al., The effect of solvent solubility parameter on turbulent
`drag reduction in polyisobutylene solutions, Experiments in Fluids,
`34, pages 535-539 (2003)
`Kim et al., Effect of Solubility Parameter of Polymer-Solvent Pair
`on Turbulent Drag Reduction, Macromol. Symp., 222, pages 169-
`174 (2005)
`Choi et al., Polymer-Induced Turbulent Drag Reduction, Ind. Eng.
`Chem. Res., 35, pages 2993-2998 (1996)
`Choi et al., Universal drag reduction characteristics of
`polyisobutylene in a rotating disk apparatus, Polymer, 40, pages
`4527-4530 (1999)
`Reply Declaration of Professor Thomas H. Epps, III (Confidential)
`LSPI LinkedIn website,
`https://www.linkedin.com/company/4788754/
`
`1080
`
`1081
`
`1082
`
`1083
`1084
`1085
`1086
`1087
`
`1088
`
`1089
`
`1090
`
`1091
`
`1092
`
`1093
`
`6
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`EXHIBIT
`1094
`
`1095
`
`1096
`
`1101
`
`1102
`
`1097
`1098
`1099
`1100
`
`DESCRIPTION
`Presentation, undated, LSPI_DRA_0036041-79 (Confidential)
`Patent Owner website for ExtremePower® Flow Improvers,
`www.liquidpower.com/applications/heavy-crude/
`Schedule and talk descriptions, LSPI_DRA_0054409-10
`(Confidential)
`Email, LSPI_DRA_0063705-06 (Confidential)
`Excel spreadsheet, LSPI_DRA_0063707 (Confidential)
`Email, LSPI_DRA_0063635-37 (Confidential)
`Email, LSPI_DRA_0063274-75 (Confidential)
`K. Solberg, Heavy-Oil Challenges: Transport, Blending, and
`Marketing, Offshore Technology Conference, 2006
`U.S. Patent No. 6,015,779 (“Eaton”)
`Yung N Lee, Ph.D., Improving Transportation of Heavy Crudes by
`Use of DRA Technology, World Heavy Oil Congress 2014
`(WHOC14-285)
`Reserved
`Transcript of the April 26, 2017 cross-examination of Brian Dunn,
`Ph.D., taken in IPR2016-00734
`Young & Lovell, Introduction to Polymers, Second Edition, 1991,
`pages 160-163
`L.H. Sperling, Introduction to Physical Polymer Science, 3rd ed.,
`2001, pages 63-70
`Plant Sheet (Confidential, Outside Attorneys Eyes Only)
`1108
`U.S. Patent No. 4,983,186 (“Naiman”)
`1109
`1110-11 Reserved
`Vargas et al., Development of a General Method for Modeling
`Asphaltene Stability, Energy & Fuels, 23, pages 1147-1154 (2009)
`
`1103
`
`1104
`
`1105
`
`1106
`
`1107
`
`1112
`
`7
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`EXHIBIT
`
`DESCRIPTION
`Vargas et al., Development of a General Method for Modeling
`Asphaltene Stability, Energy & Fuels, 23, pages 1147-1154 (2009),
`as marked by Professor Thomas H. Epps, III.
`REDACTED Transcript from August 25, 2017 cross-examination of
`Brian Dunn, Ph.D.
`REDACTED Reply Declaration of Professor Thomas H. Epps, III
`Transcript of April 13, 2018 conference call
`Declaration of Frank Niznik dated April 18, 2018
`
`1113
`
`1114
`
`1115
`1116
`1117
`
`
`
`Dated: April 18, 2018
`
`
`
`
`Respectfully submitted,
`
`/Herbert D. Hart III/
`Herbert D. Hart III
`Registration No. 30,063
`McAndrews, Held & Malloy, Ltd.
`500 West Madison Street, 34th Floor
`Chicago, Illinois 60661
`Office: (312) 775-8000
`Fax: (312) 775-8100
`Email: hhart@mcandrews-ip.com
`
`Lead Counsel for Petitioner
`Baker Hughes, a GE company, LLC
`
`8
`
`
`
`Petitioner’s Updated Exhibit List
`IPR2016-01901
`U.S. Patent No. 8,450,249 B2
`
`
`CERTIFICATE OF SERVICE
`
` I hereby certify that a true and correct copy of the foregoing
`
`PETITIONER’S UPDATED EXHIBIT LIST was served on April 18, 2018, via
`
`email to counsel for Patent Owner at the following:
`
`
`
`Douglas W. McClellan
`doug.mcclellan@weil.com
`
`Elizabeth S. Weiswasser
`elizabeth.weiswasser@weil.com
`
`Melissa L. Hotze
`melissa.hotze@weil.com
`
`
`
`
`MCANDREWS HELD & MALLOY
`
`
`
`
`
`
`Telephone: 312-775-8000
`
`
`Facsimile: 312-775-8100
`
`
`CUSTOMER NUMBER: 23446
`
`
`
`
`
`
`
`
`
`
`/Herbert D. Hart III/
`Herbert D. Hart III
`Registration No. 30,063
`
`
`
`
`9
`
`
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