`
`Petitioners' Exhibit 1012, pg. 1
`
`Petitioners' Exhibit 1012, pg. 1
`
`

`

`DIRECTORY AND DATABOOK
`
`Compiled by David l‘3ashford
`Materials Consultant
`
`ERA Technology Limited
`Leatherhead
`
`Surrey
`UK
`
`THERMOPLASTICS
`
`London -Weinheim - New York - Tokyo - Melbourne - Madras
`
`
`
`CHAPMAN 61 HALL
`
`Petitioners' Exhibit 1012, pg. 2
`
`

`

`Published by Chapman & Hall, 2-6 Boundary Row, London SE1 8HN, UK
`
`Chapman & Hall, 2~6 Boundary Row, London SE1 8HN, UK
`
`Chapman & Hall GmbI'I, Pappelallee 3, 69469 Weinheim, Germany
`
`Chapman & Hall USA, 115 Fifth Avenue, New York, NY 10003, USA
`
`Chapman & Hall Japan, ITP—Japan, Kyowa Building, 3F, 2-2-1 Hirakawacho, Chiyoda-lcu, Tokyo 102,
`Japan
`
`Chapman & Hall Australia, 102 Dodds Street, South Melbourne, Victoria 3205, Australia
`
`Chapman. & Hall India, R. Seshadri, 32 Second Main Road, CIT East, Madras 600 035, India
`
`(Permanence of Paper).
`
`Apart from any fair dealing for the purposes of research or private study, or criticism or review, as
`permitted under the UK Copyright Designs and Patents Act, 1988, this publication may not be reproduced,
`stored, or transmitted, in any form or by any means, without the prior permission in writing of the
`publishers, or in the case of reprographic reproduction only in accordance with the terms of the licences
`issued by the Copyright Licensing Agency in the UK, or in accordance with the terms of licences issued by
`the appropriate Reproduction Rights Organization outside the UK. Enquiries concerning reproduction
`outside the terms stated here should be sent to the publishers at the London address printed on this page.
`The publisher makes no representation, express or implied, with regard to the accuracy of the
`information contained in this book and cannot accept any legal responsibility or liability for any errors or
`omissions that may be made.
`
`First edition 1997
`
`© 1997 Chapman & Hall
`
`Printed in Great Britain at T]. Press (Padstow) Ltd., Padstow, Cornwall
`
`ISBN 0 412 733501
`
`A catalogue record for this book is available from the British Library
`
`C") Printed on acid-free text paper, manufactured in accordance with ANSI/NISO Z39.48—1992
`
`Petitioners' Exhibit 1012, pg. 3
`
`

`

`DATABOOK
`
`DATABOOK
`
`INTRODUCTION
`
`El Each section contains a number of data tables organized in alphabetical order by the name of the
`manufacturer.
`
`El Each data table contains a number of grades, in eight columns. A standardized format has been applied to
`the properties quoted. These can vary between the sections depending on the amount of data provided by
`manufacturers for each class of polymer.
`
`Note: All product descriptions and numerical data has been obtained from manufacturers,
`compounders and suppliers information.
`Typical examples of uses.
`
`Classed by
`Wilmer or use.
`
`manufacturers' product code.
`
`“ Tradename"
`
`‘W
`Product Ran
`A Iications:
`123DPB 456RJH 789JW
`Test
`Property
`FR
`Hi
`50% F
`Method
`
`_—-_
`We in
`Melt Fiw, MFi (g/10min) |SO1133
`Product
`Densi
`(g/cm”)
`iso 1183
`descriptors.
`(See: Key)
`
`
`This data section contains:
`a List of test method standards commonly quoted by manufacturers for their products.
`a Key to abbreviations used to describe products in the data sheets.
`[3 Key to properties listed in the data tables.
`[3 Sections (total of 17) classed in thermoplastic groups:
`. Olefins
`Page 143
`Styrenics
`Page 189
`Vinyl chlorides
`Page 227
`Fluoropolymers
`Page 237
`Acrylics
`Page 249
`Acetals
`Page 255
`Poiyamides
`Page 269
`Poiyurethanes
`Page 331
`Elastomers
`Page 339
`Polymer alloys
`Page 353
`Polyphthalamides
`Page 373
`Aromatic polyesters
`Page 377
`Aliphatic polyketones
`Page 431
`Polyarylene ethers
`Page 433
`Aromatic polyketones
`Page 443
`Sulphides/sulphones
`Page 449
`Polyimides
`Page 469
`
`Electrical
`
`ents:
`
`Key to descriptors used. Manufacturers’
`comments on grades. Other grades available.
`
`Series of properties:
`Processing
`Mechanical
`Thermal
`
`Petitioners' Exhibit 1012, pg. 4
`
`

`

`138
`
`DATABOOK
`
`LIST OF TEST METHOD STANDARDS
`
`Those listed are commonly quoted by material manufacturers’ and appear in the data tables.
`
`
`Property
`
`Units
`
`International
`
`J
`
`American m
`
`
`PROCESS AND PHYSICAL PROPERTIES
`
`g/ 10 min
`Melt Flow Index, MFI
`g/cm3
`Density
`Moisture Absorption, 23°C/50%RH %
`Water Absorption, 24 hours
`%
`Water Absorption, saturated
`%
`Mould Shrinkae
`°/o
`
`ISO 1133
`ISO 1183
`ISO 62A
`ISO 62A
`ISO 62A
`ISO 2557
`
`DIN 53735
`ASTM D 1238
`DIN 53479
`ASTM D 792
`DIN 53495
`ASTM D 570
`DIN 53495
`ASTM D 570
`DIN 53495
`ASTM D 570
`
`ASTM D 955
`-
`
`
`MECHANICAL PROPERTIES
`
`Tensile Modulus
`UTS (or YS)
`Elongation
`Flexural Modulus
`Flexural Strength
`Compressive Strength
`Shear Strength
`Tensile roerties offilms
`
`GPa (or MPa)
`MPa
`°/o
`GPa (or MPa)
`MPa
`MPa
`MPa
`—
`
`ISO 527
`ISO 527
`ISO 527
`ISO 178
`ISO 178
`ISO 604
`-
`-
`
`ASTM D 638
`ASTM D 638
`ASTM D 638
`ASTM D 790
`ASTM D 790
`ASTM D 695
`ASTM D 732
`ASTM D 882
`
`DIN 53457
`DIN 53455
`DIN 53455
`DIN 53452
`DIN 53452
`DIN 53454
`-
`-
`
`
`IMPACT PROPERTIES
`
`Impact Strength (Izod)
`Notched Impact Strength (Izod)
`Impact Strength (Charpy)
`Notched Impact Strength (CharPY)
`Tensile Impact Strength
`Free Falling Dart Drop Test
`Instrumented Dart Test
`
`ISO 180/1C
`ISO 180/1A
`ISO 179/1 D
`ISO 179/1A
`ISO 8256
`-
`—
`
`—
`—
`
`ASTM D 256 (J/m)
`ASTM D 256 (J/m)
`-
`-
`ASTM D 1822
`ASTM D 1709
`ASTM D 3763
`
`-
`-
`DIN 53453
`DIN 53453
`DIN 53448
`—
`—
`
`
`THERMAL AND PERFORMANCE PROPERTIES
`
`DIN 53460
`DIN 53461
`-
`DIN ISO 2039
`DIN 53505
`DIN 53505
`DIN 53752
`-
`DIN 53754/53516
`—
`-
`
`-
`-
`
`the individual test standard.
`
`
`
`'
`
`Vicat Softening Point
`Heat Distortion Temperature
`Flammability
`Rockwell Hardness
`Shore Hardness
`Durometer Hardness
`Coefficient of Thermal Expansion
`Tear Strength
`Abrasion Resistance
`Limiting Oxygen Index
`Continuous Use Temperature
`Thermal Conductivity
`Coefficient of Friction
`Environmental Stress Cracking
`Resistance ESCR
`
`°C
`r‘C
`Rating, mm
`-
`-
`-
`10£l°C
`N/mm
`mm3
`%
`°C
`W/m
`-
`—
`
`ISO 306
`ISO 75
`UL 94
`ISO 2039
`ISO 868
`-
`-
`—
`-
`ISO 4589
`—
`—
`-
`-
`
`ASTM D 1525
`ASTM D 648 (HDUL)
`UL 94
`ASTM D 785
`ASTM D 2240
`ASTM D 2240
`ASTM D 696
`ASTM D 1004/1922
`ASTM D 1044/1242
`ASTM 2863
`UL746A
`ASTM C 177
`ASTM D 1984
`ASTM D 1693 for
`polyethylene
`
`ELECTRICAL PROPERTIES
`
`Dielectric Strength
`Volume Resistivity
`Surface Resistivity
`Dielectric Constant
`Dissipation Factor
`Comparative Tracking Index
`Arc Resistance
`
`kV/mm
`Q.cm
`Q
`-
`-
`V
`sec
`
`ISO 1325 / IEC 243-1 ASTM D 149
`ISO 1325 / IEC 93
`ASTM D 257
`ISO 1325 / IEC 93
`ASTM D 257
`IEC 250
`ASTM D 150
`ISO 1325 / IEC 250
`ASTM D 150
`DIN 53480
`—
`IEC112A
`ASTM D 495 DIN 53484
`
`-
`
`DIN 53481
`DIN 53482
`DIN 53482
`DIN 53483
`
`Note: Units apply to International Standards, where National Standards apply different units these are given in brackets for
`
`Petitioners' Exhibit 1012, pg. 5
`
`

`

`DATABOOK
`
`Properties and Abbreviations 139
`
`KEY TO DATA SHEETS AND PROPERTIES
`
`LWVP = low water vapour
`permeability
`MF = mineral filler
`
`MFFR = migration free flame
`retardant
`
`MG = mixed glass
`MGF = milled glass fibre
`Ml = medium impact
`mod. = modified grade
`MPG = micronized powder grade
`MR = mould release
`
`MV = medium viscosity
`NA = non-automobile
`
`NCGF = nickel coated graphite
`fibre
`
`NFF = non-free flowing
`P = plasticizer addition
`PC = petroleum coke
`PE = paste extrusion
`P-free = phosphorous free
`PG = powder grade
`RC = recyclate
`RCO = random copolymer
`reinf. = reinforced grade
`SC = soft carbon
`
`SCC = super conductive carbon
`SD = static dissipation
`SE = self extinguishing
`SF = special filler
`SG = standard grade
`SHl = super high impact
`Sl = silicate filler
`Si = silicone addition
`
`SlG = super impact grade
`SL = self-lubricated
`
`SP = suspension polymer
`Special = grade (as indicated)
`SPG = special grade
`SSF = stainless steel fibres
`
`ST = super tough
`Surface = good surface finish
`Susp = suspension
`T = toughened
`TFE = tetrafluoroethylene lubricant
`TG = transparent grade
`TR = translucent
`Trans = transparent
`Unfilled = no filler, i.e.
`unreinforced
`UV = UV stabilized
`
`VHF = very high flow
`VHl = very high impact
`VM = vacuum metallization
`Wh = whisker reinforcement
`
`WP = white pigment
`
`Co = copolymer
`cond = conductive
`
`CP = conductive pigment
`CPG = chrome plate grade
`Cu = copper
`decor = decorative grade
`DP = dispersion powder
`DS = dimensional stable
`EA = external automobile
`
`Econ = economy grade
`EF = easy flow
`EG = electrical grade
`EL = elastomer addition
`
`ELV = extremely low viscosity
`EMl = electromagnetic shielding
`emul = emulsion
`
`EP = electroplatable
`ESCR = environmental stress
`
`cracking resistance
`ET = extra toughness
`FC = fast cycle
`FF = free flowing
`FG = food grade
`filled = filled grade
`Foam = foamed sheet (food
`packaging)
`FR = flame or fire retardant
`
`G = mineral glass
`G-WR = glow-wire rated
`GB = glass beads
`GF = glass fibres
`GP = general purpose
`Gr = graphite
`GS = glass spheres
`H = halogenated
`HD = heat deformation resistance
`
`HF = halogen free
`HG = high gloss
`HH = high heat
`HI = high impact
`HIF = high flow
`HIM = high modulus
`HIS = high strength
`HlT = high toughness
`HMA = hot melt adhesive
`
`Ho = homopolymer
`HR = heat resistant
`HS = heat stabilized
`
`HSCR = high stress cracking
`resistance
`
`HV = high viscosity
`IG = impact grade
`IM = impact modified
`LF = low friction
`
`LG = low gloss (matt)
`LGF = long glass fibres
`LOF = low melt flow
`LOT = low temperature
`Lub = lubricated
`LV = low viscosity
`LW = low warpage
`
`bm = blow moulding
`cable ext = cable extrusion
`cal = calendaring
`cm = compression moulding
`couext = co-extrusion
`dm = dip moulding
`as = electrostatic coating
`ext = extrusion
`fibre = grade for fibre manufacture
`fila = for filament manufacture
`film = for film manufacture
`im = isostatic moulding
`inj = injection moulding
`mg = moulding grade (used where
`the processing options have
`not been defined, but usually
`implied as injection moulding)
`pa = paste extrusion
`rot = rotational moulding
`sol = processed by solution
`tf = thermoforming
`tm = transfer moulding
`vf = vacuum forming
`
`WR = weather resistance
`
`ABBREVIATIONS
`
`Processing
`
`Descriptors/Comments On
`Grades
`
`Note: These apply to descriptors
`in data tables (given in not bold,
`capital letters after manufacturers’
`product code). They do not apply
`to designations within the grade
`description, as given by the
`manufacturer, unless specifically
`stated in the comment box.
`
`uwave = microwave (food
`packaging)
`Add-free = additive free
`ADQ = aqueous suspension
`polymer
`AF = aramid fibres
`Anti-F = anti-friction
`AP = automotive paint receptive
`AR = arc resistance
`AS = anti~static
`3C0 = block copolymer
`BG = bearing grade
`Br = bronze
`Br-free = no bromine additives.
`BS = barium sulphate
`CB = carbon black
`CC = chemically coupled
`CD = coagulated dispersion
`CF = carbon fibres
`CK = chalk filler
`
`Petitioners' Exhibit 1012, pg. 6
`
`

`

`140 Properties and Abbreviations
`
`DA TABOOK
`
`PROPERTIES
`
`Applies to properties in the data tables. Abbreviations have been used in the tables owing to the length of some
`terms.
`
`Processing Various abbreviations are used in the data tables to indicate the intended process route for
`individual grades of polymer (See: Abbreviations - Processing).
`
`Melt Flow, MFl Melt Flow Index is a parameter which describes the basic flow characteristics of a polymer. It
`is measured at a temperature appropriate to the polymer and under a defined load, e.g. 210°Cl5.0 kg.
`Data can be quoted without the test conditions, in these cases the numbers allow relative comparisons
`between grades. A high MFl value indicates a material suitable for moulding thin sections, whilst low
`values tend to indicate extrusion grades.
`
`for engineering applications.
`
`Density A physical characteristic of all materials quoted at 23°C. Differences in quoted densities across a
`range of like polymers may indicate the addition of fillers,
`reinforcing fibres or flame retardants.
`Variations on crystalline and amorphous microstructures can induce density differences.
`
`This parameter describes the mass increase of dry material when conditioned at
`Moisture Absorption
`50% RH. and 23°C. Absorbed moisture levels can affect processing, where less than 0.2% is usually
`required to ensure acceptable moulding surface finish. Some polymers, with high absorbed moisture
`levels, need drying before processing.
`
`Water Absorption A measurement of the mass increase of dry material when immersed in water at 23°C.
`Water absorption levels can be quoted for 24 hours immersion or until full saturation has occurred.
`
`Mould Shrinkage A measurement of the contraction of the moulded material in comparison with the original
`mould dimensions. Two values may be quoted where material flow induces anisotropy in material
`microstructure, e.g. preferential alignment of reinforcing phases. Example: 2.0/3.0 indicates 2.0 %
`shrinkage in direction of material flow, with 3.0% shrinkage transverse to mould flow direction.
`
`Tensile Modulus Also referred to as Young’s modulus or modulus of elasticity in tension. it is a measure of
`the slope of the stress against strain plot for small extensions within the region where the material is still
`demonstrating elasticity. Modulus is given in GPa.
`In the data tables values in MPa are only used for
`elastomers. Note: Manufacturers can quote modulus in MPa or N/mmz.
`
`in MPa, is the stress obtained at the point of material failure. For plastics, the
`UTS Ultimate tensile strength,
`testing speed and temperature influences the value obtained. For lower modulus plastics with high
`strain to failure, the stress at failure can be lower than the yield stress. In the data tables the highest
`stress value obtained by the test is given.
`
`YS
`
`is the stress at the yield point when the material departs from elasticity by a
`in MPa,
`Yield strength,
`specified limiting deviation from the proportionality of stress to strain. Low strain to failure plastics often
`do not have a quotable yield stress, so UTS is quoted instead.
`
`Elongation Used to describe the elongation at break or strain to failure of a material as a percentage of the
`original material length. For thermoplastics, the range can go from ~1% for a highly filled material to
`>500% for an elastomer.
`
`Flexural properties are usually measured in order to obtain a measure of stiffness or
`Flexural Modulus
`rigidity. As with tensile properties. flexural modulus, in GPa, depends on the testing temperature. The
`flexural modulus of elastomers is quoted in MPa.
`
`Flexural Strength Also known as breaking strength, the value quoted in MPa, can be either at rupture or yield
`depending on the type of material.
`
`Compressive Str Compressive strength or crushing strength,
`performance thermoplastics for engineering applications.
`
`in MPa,
`
`is occasionally quoted for the higher
`
`Shear Str Shear strength, in MPa, is occasionally quoted with the higher performance thermoplastics intended
`.
`
`Petitioners' Exhibit 1012, pg. 7
`
`

`

`DA TABOOK
`
`Properties and Abbreviations 141
`
`[5 Izod Unnotched Izod Impact Strength. The test uses a rectangular bar, which is often injection moulded.
`One end of the bar is clamped, the sample is struck by a pendulum, with the free-end fractured by the
`impact. The value obtained is the energy required to break a specified area of material,
`in kJ/mmz.
`Historically, the value can also be quoted in Joules per metre (J/m). Some flexible polymers do not
`fracture under test and in such cases a ‘No break‘ result is given. Impact properties are usually quoted
`at 23°C and at a lower temperature (between -20°C and -40°C) where a rubbery-to-brlttle transition
`could occur at a low service temperature.
`
`Notched Izod Impact Strength, The notch is either moulded into the bar, or machined (more
`N13 Izod
`reproducible). Notching a sample allows an understanding of the materials behaviour changes in
`section induce stress concentrations. Some polymers are notch sensitive. Impact properties are usually
`quoted at 23°C and at a lower temperature (between -20°C and -40°C) where a rubbery-to-brittle
`transition could occur in the polymer at a low service temperature.
`
`[3 Charp Unnotched Charpy Impact Strength. The Charpy impact test uses a rectangular bar which is struck
`by a pendulum or hammer (or tup). The value obtained is given as the energy required to break a
`specified area of material,
`in kJ/mmz. Specimen preparation is similar to that used for the Izod test
`although the test itself is markedly different to the Izod test as both ends of the sample are unclamped.
`
`NIS Charp Notched Charpy Impact Strength. As with the Izod test, results at 23°C and between -20°C and
`-40°C are usually given. The notch dimensions for Charpy specimens differ to those used in Izod tests.
`
`Vicat Vicat Softening Point (VSP). A thermal softening point test performed using a Vicat needle instrument,
`quoted in °C. It is measured by applying a standard load, either 10 or 5ON, via a circular indentor onto a
`specimen. The sample is heated at a constant rate until the indentor sinks into the sample by a set
`distance. The result is quoted with respect to the load applied and temperature.
`
`(vary with direction) to some extent, This is affected by processing and by reinforcement orientation.
`
`the highest rating; where the specimen burns for less than 10 seconds after either of two
`applications of a defined Bunsen flame. Total flaming combustion time of less than 50 seconds
`for 10 flame applications on five specimens, with no ignition of the surgical cotton.
`V1: specimen burns for less than 30 seconds after either application of the test flame. Total flaming
`combustion time of less than 250 seconds for 10 flame applications on five specimens, with no
`ignition of the surgical cotton.
`V2: as for V1, but flaming particles may occur that ignite the surgical cotton.
`HB: the lowest rating; where the combustion speed is less than 38 mm/min.
`
`Heat Distortion Temperature, or heat deflection under load (HDUL). A three-point flexural test is
`performed on a bar by applying a load to create a stress of either 1.80 MPa or 0.45 MPa at the mid-
`point. The temperature is raised by a predetermined rate and when the specimen deflects by a set
`amount, the temperature is quoted, in °C.
`
`Flammability The flammability of a plastic is most commonly characterised by the Underwriters Laboratory
`(UL 94) horizontal burning test. The test sample, a rectangular bar 127 mm long, is held horizontally, or
`at 45°, and clamped at one end. The burning speed of the bar
`is measured when exposed to a pilot
`flame. The bar is held 305 mm above the surface of a layer of surgical cotton. The thickness of the bar
`can be varied, but is quoted as part of the result, e.g. V0, 1.57. The commonly quoted ratings given to a
`material are:
`
`V0:
`
`A number which indicates the hardness of a material as measured by an standard
`Rockwell Hardness
`indentation test. The use of different loads and indentors gives several Rockwell hardness scales; R
`and M are commonly applied to plastics.
`
`Shore Hardness A measure of the hardness, or softness, of a material as assessed by the resistance (on a
`scale of 0 to 100) to a loaded indentor. 100 corresponds to a high resistance and 0 to zero resistance.
`Two different scales are used for plastics; Shore A (soft materials) or Shore D (harder materials).
`
`CTE Coefficient of Thermal Expansion describes the amount by which a material expands for each degree rise
`in temperature. Thermoplastics have higher CTE values than metals, typically in the range 50 to 150 x
`10'6°/C. The addition of fillers and reinforcements reduces these values. Expansion may be anisotropic
`
`Petitioners' Exhibit 1012, pg. 8
`
`

`

`Volume Res Volume Resistivity (internal resistivity, formerly specific resistance) is used to characterise the
`insulation behaviour of plastics and elastomers.
`It is usually given at 0°C or 20°C. Materials with a
`volume resistivity >108 ohm.cm are classed as insulators (plastics or elastomers). Materials are anti-
`static in the range 102 to 108 ohm.cm. Conducting polymers are <102 ohm.cm.
`
`Surface Res Surface Resistivity is measured as the resistance, in ohms, on opposite edges of a square of a
`material. The size of the square is immaterial as increasing the size increases the width of the
`conductive path but also lengthens it in proportion.
`
`(sometimes specific inductive capacity or
`relative permittivity,
`Dielectric Constant, or
`Dielect Const
`permittivity) is a measure of how well a material will store electrical charge. An insulating material needs
`a low dielectric constant. It is the (unitless) ratio of the capacity of a condenser made with a plastic over
`the capacity of an identical condenser made with air as the dielectric.
`
`Diss Factor Dissipation Factor and power factor are the same for most dielectrics (insulators) and are a
`measure of how much power is converted to heat. Values may be quoted in two ways, eg. 0.002 or
`20 x 10'“. Heat conversion is undesirable in an insulator and so the power factor should be as low as
`possible.
`
`CTI Comparative Tracking Index. A test used to assess materials for their resistance to surface tracking when
`subjected to an electric stress in a wet environment. The result is expressed as the maximum voltage
`(in Volts) at which tracking does not occur when 50 drops of an ionic solution (salt solution of 0.1%
`ammonium chloride) are applied to the active region of test specimen.
`
`Arc Resistance Tests performed to determine the resistance of a polymer compound to electric arcs such as
`
`142 Properties and Abbreviations
`
`DA TABOOK
`
`Tear resist Tear resistance or tear strength is the force required to propagate a rip, or tear, in a material, given
`in N/mm. The tearing energy is usually expressed as the ratio of the maximum load measured during
`the test to the specimen thickness. This parameter is applicable to materials used for film or sheet
`applications; also elastomers.
`
`Abrasion resist The abrasion resistance of a material is measured by wearing away a surface in contact with
`a moving abrasive surface. This test is usually applied to rubbers and elastomers, with the value
`expressed in cubic millimetres (mm3) of material removed after a defined period.
`
`Dielectric Str Dielectric Strength (Electric Strength) is the maximum potential gradient that can be applied to a
`material without causing it to break down (usually expressed in kV/mm).
`it is a measure of how well a
`material, a dielectric, can withstand a voltage. The resistance to dielectric breakdown is specified as the
`voltage at which breakdown occurs divided by the specimen thickness. Breakdown occurs as a sudden
`flow of current through the material, Specimen thicknesses are usually >3 mm.
`
`appear in high voltage switch-gear and in circuit breakers.
`
`Petitioners' Exhibit 1012, pg. 9
`
`

`

`poL YACETALS
`“Hostaform C” Copolymer
`Hoechst AG
`A lications: Automotive arts, electrical/electronic, telecommunications, com uters, ear wheels, slidin arts.
`9021
`Property
`Test
`32021
`32021
`52021
`9021
`9021 ELS
`9021 G
`9021
`GV1 I40
`Method
`Unfilled
`AST
`Unfilled
`UnfiIIed
`HI
`UnfiIIed
`GV1/30
`
`Unfilled
`Unfilled
`26%GF
`40%GF
`
`Acetals (POM) 259
`, POM
`
`inj, ext
`3.8
`
`inj
`5.5
`
`.
`
`inj
`2.7
`
`inj
`27
`
`inj
`29
`
`inj
`40
`
`inj, ext
`8.5
`
`inj
`4
`
`.
`
`.
`
`ISO180/1A
`
`(°C)
`(“0)
`
`'30 1325
`
`“Hostaform C” Copolymer
`,
`Hoechst AG
`A Iications: Automotive arts, electrical/electronic, telecommunications, comuters, ear wheels, slidin arts.
`1020
`Property
`Test
`9021
`9021
`9021
`9021 HL
`9021 K
`9021 M
`9021 TF
`Method
`GV3/10
`GV3/20
`GV3I30
`BLACK with chalk Unfilled with PTFE Unfilled
`10%GS
`20%GS
`30%GS
`10I1569*
`
`POM
`
`Melt Flow MFI (g/10 min) ISO 1133
`190°C / 2.15 k
`1.41
`1.52
`1.42
`1.44
`1.41
`1.59
`1.53
`1.47
`(g/cm‘) Iso 1183
`Density
`0.2
`0.2
`0.2
`0.2
`0.2
`0.12
`0.15
`0.15
`Moisture Absorption (%) DIN 53495
`-
`—
`-
`—
`-
`—
`-
`-
`Mould Shrinkage
`(%) -
`2.6
`2.4
`2.7
`2.9
`2.8
`3.7
`3.4
`3.1
`Tensile Modulus
`(GPa)
`ISO 527
`63 (Y8)
`49 (Y8)
`64 (Y8)
`62 (Y8)
`64 (Y8)
`41 (Y8)
`47 (Y8)
`54 (YS)
`UTS (orYS)
`(MPa)
`ISO 527
`35
`20
`28
`25
`25
`15
`18
`20
`Elongation
`(%)
`ISO 527
`No break
`42
`100
`70
`95
`18
`27
`38
`Is Izod, 23°C
`(kJ/m‘)
`ISO 180/1C
`135
`42
`85
`70
`70
`18
`27
`38
`-30°C
`7.0
`3.0
`5.0
`4.0
`5.0
`3.0
`3.0
`3.5
`NIS Izod, 23°C (kJ/mz)
`6.0
`3.0
`5.0
`4.0
`5.0
`2.5
`3.0
`3.2
`~30°C
`150
`145
`150
`150
`150
`151
`151
`151
`ISO 306
`Vicat B, 50 N
`97
`98
`100
`100
`105
`112
`110
`108
`ISO 75
`HDT, 1.8 MPa
`HB,1.57 HB,1.57 HB,1.57 HB,1.57
`-
`HB,1.57 HB,1.57 HB,1.57
`UL 94
`Flammability,mm
`120
`120
`120
`130
`120
`110
`100
`90
`CTE, 23/80°C (108°C) DIN 53752
`35
`35
`33
`28
`28
`35
`35
`4O
`Dielect Str
`(kV/mm) IEC 243-1
`1014
`10‘4
`1o“
`10‘4
`1014
`1014
`10‘4
`10‘4
`Volume Res
`(eom) IEC 93
`1014
`10‘4
`1014
`10‘4
`10‘4
`10”
`10‘4
`1014
`Surface Res
`(9)
`IEC 93
`4.2
`4.2
`4.0
`4.1
`—
`4.3
`4.5
`5.0
`Dielect const @ 50 Hz
`IEC 250
`4.5
`4.5
`4.4
`4.6
`-
`4.7
`4.7
`5.0
`@1 MHz
`0.0065
`0.0085
`0.0087
`0.0026
`-
`0.026
`0.04
`0.8
`Diss Factor @ 50 Hz
`0.23
`0.18
`0.21
`0.16
`-
`0.21
`0.23
`0.23
`@1 MHZ
`600
`600
`600
`600
`300
`600
`600
`600
`IEC112
`(V)
`CTI
`Comments: GS = glass spheres. bm = blow moulding, * Light and weather stabilised.
`
`lso 180/1A
`
`(°C)
`(°C)
`
`ISO 1325
`
`inj, ext,
`bm
`0.8
`
`
`
`Processing
`Melt Flow MFI(g/10 mln) ISO 1133
`190°C / 2.16 k
`1.72
`1.41
`1.41
`1.41
`1.41
`ISO 1183
`(g/cm“)
`Density
`0.14
`0.2
`0.2
`0.2
`0.2
`Moisture Absorption (%) DIN 53495
`-
`-
`-
`-
`-
`Mould Shrinkage
`(%) —
`13.0
`9.0
`2.3
`1.9
`2.8
`2.9
`2.8
`2.9
`Tensile Modulus
`(GPa)
`ISO 527
`115
`115
`43 (Y8)
`35 (YS)
`64 (YS)
`65 (YS)
`64 (Y8)
`64 (YS)
`ms (or YS)
`(MPa)
`ISO 527
`
`Elongation
`(%)
`ISO 527
`25
`25
`18
`32
`30
`12
`3.0
`2.0
`)5 Izod, 23°C
`(kJ/mz)
`ISO 180/10
`90
`85
`80
`130
`85
`20
`25
`16
`-30°C
`80
`80
`70
`100
`35
`20
`28
`18
`N15 Izod, 23°C (kJ/mz)
`5.0
`5.0
`4.0
`5.5
`4.5
`3.0
`4.5
`4.5
`
`“30°C
`5.0
`5.0
`4.0
`5.5
`2.0
`3.0
`5.0
`5.0
`ISO 306
`Vicat B, 50 N
`151
`151
`151
`151
`130
`140
`158
`160
`ISO 75
`HDT, 1.8 MP5
`106
`100
`106
`104
`89
`88
`160
`161
`UL 94
`Flammability , mm
`HB, 1.57
`HB, 1.57 HB, 1.57 HB, 1.57
`-
`-
`HB, 1.57 HB, 1.57
`
`GTE, 23/80°C (10‘6/°C) DIN 53752
`120
`120
`120
`120
`130
`140
`30
`10
`Dielect Str
`(kV/mm) IEC 243-1
`35
`-
`35
`35
`-
`35
`40
`40
`Volume Res
`(eom) IEC 93
`1o”
`3 x1013
`1014
`1o”
`103
`10”
`10‘4
`1014
`Surface Res
`(:2)
`IEC 93
`10‘4
`10“
`1014
`10‘4
`5 x103
`10”
`1014
`1014
`Dielect const @ 50 Hz
`IEC 250
`4.0
`—
`4.0
`4.0
`-
`3.8
`4.5
`4.7
`@ 1 MHZ
`4.4
`—
`4.4
`4.4
`4.4
`5.0
`5.7
`0335 Factor @ 50 HZ
`0.005
`0.0056
`0.004
`0.007
`0.005
`0.011
`@1 MHZ
`0.17
`0.17
`0.17
`0.2
`0.23
`0.28
`IEC112
`(V)
`600
`600
`600
`600
`600
`600
`CTI
`Comments: AST = anti-static. IM = impact modified, GF = glass fibres.
`
`See Key to Data Sheets - Pages 139 to 142
`
`
`Processing
`
`inj
`
`inj
`
`in)
`
`in}
`
`inj
`
`inj
`
`inj
`
`10
`
`9.0
`
`7.0
`
`8.5
`
`8.0
`
`8.5
`
`6.7
`
`
`
`Petitioners' Exhibit 1012, pg. 10
`
`

`

`AROMA TIC POL YESTERS
`
`
`Polyethylene Terephthalates (PET) 397
`
`“Eastapak & Eastar”
`Eastman Chemical Company
`Applications: Carbonated beverages, food, water, cosmetics, pharmaceuticals.
`
`PET & PETG
`'
`
`Property
`
`Test
`Method
`
`Processing
`Melt Flow MFI (9/10 min) ISO 1133
`Density
`(g/cm’)
`D1505
`
`5214A
`Bright
`amber
`bm
`—
`1.40
`14959
`Co—
`polyester
`
`9663
`Clear
`
`bm
`-
`1.40
`15086
`PETG
`
`9921W 9922W
`Clear
`Clear
`
`9980R
`Clear
`
`12440
`Clear
`
`13213
`Emerald
`
`13339
`Clear
`
`hm
`—
`1.40
`
`hm
`—
`1.40
`Eastar
`6763
`PETG Co-
`ol ester
`
`—
`1.40
`Eastar
`DN004
`PCTG
`
`Eastar
`GN007
`PETG
`
`Eastar
`EN003
`Co—
`
`Eastar
`EN058
`
`—
`1.27
`
`5O (YS)
`110
`2.1
`
`-
`1.33
`—
`58 (YS)
`100
`2.5
`
`high flow
`1.33
`
`62 (YS)
`14
`2.7
`
`—
`52
`330
`1.8
`
`-
`-
`No break
`_
`
`-
`101
`_
`
`-
`50 (YS)
`130
`2.1
`70
`No break
`No break
`101
`37
`
`See Key to Data Sheets - Pages 139 to 142
`
`ISO 306
`(“0)
`Vicat B, 50 N
`(°C) ISO 75
`HDT, 1.8 MPa
`Flammability , 1.6 mm
`UL 94
`CTE, 23/80“C (10'6/°C) DIN 53752
`DielectStr
`(kV/mm)
`IEC 243-1
`Volume Res
`(9cm)
`IEC 93
`Surface Res
`(9)
`IEC 93
`Dielect const @ 50 Hz
`IEC 250
`@ 1 MHz
`0.0097
`0,0092
`Diss Factor @ 50 Hz
`0.016
`0.019
`0.02
`@1 MHZ
`275
`275
`275
`lEC112
`(V)
`CTI
`Comments: Grades have 20, 30 & 45% glass fibres respectively. All heat stabilised.
`
`Processing
`Melt Flow MFI (9/10 min) ISO 1133
`Density
`(g/cm’)
`D1505
`Tensile Modulus (GPa) D638
`UTS (or YS)
`(MPa) D638
`Elongation
`(%) D638
`Flexural Modulus (GPa) D790
`Flexural Strength (MPa) D790
`IS Izod, 23"C
`(J/m)
`~40°C
`NIS Izod, 23°C
`-40°C
`HDT, 1.8 MPa
`Rockwell Hardness
`
`.
`(J/m)
`
`(°C)
`
`0648
`D785
`
`Comments: Renamed products, previously Kodapak. All Eastar grades are clear, transparent and high gloss.
`Grades vary on intrinsic viscosity, molecular weight, crystalline peak melting point.
`
`“Impet”
`Hoechst AG
`Applications: Automotive, fan impellers, terminals, coil bobbins, domestic appliances, telecommunications, keyboards.
`
`PET
`
`Property
`
`Test
`Method
`
`2600
`GV1/20
`
`2600
`GV1/30
`
`2600
`GV1/45
`
`
`
`inj
`24
`
`inj
`
`inj
`3
`
`Processing
`Melt Flow MFI (g/10 min) ISO 1133
`265°C / 2.16 k
`ISO 1183
`(g/cm“)
`Density
`Moisture Absorption (%) DIN 53495
`Mould Shrinkage
`(%) -
`Tensile Modulus
`(GPa)
`ISO 527
`UTS (or YS)
`(MPa)
`ISO 527
`Elongation
`(%)
`ISO 527
`IS Izod, 23°C
`(kJ/mz)
`ISO 180/1C
`~30°C
`NIS Izod, 23°C (kJ/mz) ISO 180/1A
`-30°C
`
`
`
`
`
`
`
`ISO 1325
`
`Petitioners' Exhibit 1012, pg. 11
`
`

`

`AROMA TIC POL YESTERS
`
`Polybutylene Terephthalates (PBT) 409
`
`GE Plastics
`A Iications: Steam irons, a liance housins.
`9731
`865
`30%GF
`30%GF
`
`FR HS
`FR
`
`DR48
`15%GF
`FR HS
`
`HV7065
`65%MF
`
`HV7075
`65%MF
`
`V PBT
`
`ISO 1183
`[80 62A
`
`(°C)
`(°C)
`
`IEC 250
`
`IEC112A
`
`Diss Factor
`
`CTI
`
`70
`
`140
`120
`
`150
`67
`
`110/80
`
`90/100
`
`40/100
`
`185
`V0, 0.89
`35/v
`19
`>1O15
`2x1014
`3.6
`
`>1015
`1014
`
`0.012
`
`0.02
`
`0.02
`0.0019
`
`600
`300
`175
`300
`h im act, MF = mineral filler.
`
`Hoechst AG
`
`“Celanex”
`
`A lications: Automotive, Electrical, Sports goods, Office equipment, Telecommunications.
`2300
`2300
`2300
`Test
`2002-3
`1600A
`1700A
`2003-2
`2000-2
`Property
`No filler
`GV1/30
`Method
`No filler
`No filler
`No filler
`No filler
`GV1/10
`GV1/20
`20%GF
`30%GF
`10%GF
`
`inj, ext
`10
`
`inj, ext
`5
`
`in]
`65
`
`in}, ext
`25
`
`inj
`55
`
`
`
`DR51
`PKG153O VX5022
`Unfilled
`15%GF
`20%GF
`HI HS
`HS
`film, ext
`Processing
`inj
`in}
`in]
`in}
`mi
`inj
`inj
`13
`8
`15
`14
`-
`7
`13
`30
`Melt Flow MFI (g/10 min) ISO 1133
`
`(Temp.°C /Load. kg)
`(250/216) (250/216) (260/216) (260/216) (250/2161 (25012.16
`(265/12)
`-
`1.22
`1.41
`2.4
`2.5
`1.51
`1.39
`1.66
`1.58
`Density
`(g/cm’)
`0.07
`0.06
`0.07
`0.02
`0.05
`0.03
`—
`Moisture Absorption (%)
`0.1
`0.07
`0.15
`~
`0.04
`Water Absorption
`(%)
`
`ISO 2557
`Mould Shrinkage
`(%)
`ISO 527
`6.5
`4.9
`6.6
`10.0
`8.5
`Tensile Modulus
`(GPa)
`ISO 527
`104
`32
`45
`130
`110
`UTS (or YS)
`(MPa)
`2 2
`
`ISO 527
`2
`2
`1
`3.5
`Elongation
`(%)
`ISO 180/1C
`40
`25
`12
`50
`55
`50
`IS Izod, 23°C
`(kJ/m’)
`-30°C
`40
`25
`55
`45
`12
`25
`ISO 180/1A
`NIS Izod, 23°C (kJ/mz)
`
`-30°C
`ISO 305
`238
`188
`194
`Vicat, 50 N
`ISO 75
`85
`200
`197
`HDT, 1.8 MPa
`UL 94
`Flammability, mm
`V0, 0.78
`V0, 1.57
`DIN 53752
`25/-
`35/100
`CTE
`(10‘6/°C)
`IEC 243—1
`Dielect Str
`(kV/mm)
`IEC 93
`Volume Res
`(Q.cm)
`IEC 93
`Surface Res
`(Q)
`IEC 250
`Dieleot const @ 50 Hz
`@ 1 MHz
`@50Hz
`@1MHz
`(V)
`Comments: FR = flame retardant, HS = heat stabilized, HI = hi
`
`See Key to Data Sheets - Pages 139 to 142
`
`
`
`ISO 1183
`DIN 53495
`DIN 53495
`
`Processing
`Melt Flow MFI (g/10 min) ISO 1133
`250°C / 2.16 k
`(g/cms)
`Density
`Moisture Absorption (%)
`Water Absorption
`(%)
`Mould Shrinkage
`(%)
`Tensile Modulus
`(GPa)
`UTS (or YS)
`(MPa)
`Elongation
`(%)
`IS Izod, 23°C
`(kJ/mz)
`-30"C
`
`ISO 527
`ISO 527
`ISO 527
`ISO 180l1C
`
`Diss Factor
`
`ISO 1325
`
`1.3
`1.3
`1.3
`1.3
`1.30.25
`0.25
`0.25
`0.25
`0.25
`0.6
`0.6
`06
`0.6
`0.6
`
`2.5
`2.5
`2.5
`2.5
`2.5
`55 (YS)
`56 (YS)
`52 (YS)
`53 (YS)
`56 (YS)
`>50
`>50
`>50
`30
`>50
`70
`120
`100
`No break No break
`100
`80
`160
`No break
`70
`ISO 180/1A
`5.5
`5.0
`6
`6.5
`NIS Izod, 23°C (kJ/m‘)
`
`-30°C 4.5 6 6.5 5.5
`
`
`
`ISO 306
`195
`185
`182
`190
`Vicat B, 50 N
`(“0)
`ISO 75
`55
`55
`50
`50
`HDT, 1.8 MPa
`(°C)
`UL 94
`Flammability , mm
`HB, 1.55
`HB,1.55 HB, 1.55
`HB, 1.55
`DIN 53752
`130
`130
`130
`130
`CTE, 23/80°C (10'6/°C)
`IEC 243-1
`23
`23
`23
`23
`Dielect Str
`(kV/mm)
`IEC 93
`Volume Res
`(0cm)
`>1015
`>1015
`>1015
`>1015
`IEC 93
`>1015
`Surface Res
`(0)
`>1015
`>1015
`>1015
`IEC 250
`4.0
`4.0
`4.1
`Dielect const @ 50 Hz
`3.5
`3.5
`3.5
`@ 1 MHz
`36
`0.0014
`0.0014
`0.0014
`0.0014
`@50 Hz
`0.022
`0.026
`0.021
`0021
`@1MH2
`|EC112
`CTI
`
`600 600 600 600
`
`
`(V)
`Comments: GF = lass fibres.
`
`
`
`Petitioners' Exhibit 1012, pg. 12
`
`

`

`410 Polybutylene Terephtha/ates (PBT)
`
`AROMA TIC POL YESTERS
`
`3:31-
`
`'
`
`2360 FL
`Unfilled
`
`2360
`GV1/10
`FL
`10% GF
`
`“Celanex”
`Hoechst AG
`A lications: Automotive, Electrical, Sorts oods, Office e uiment, Telecommunications.
`Property
`Test
`2300
`2300
`2300
`2302
`2302
`Method
`GV1/50
`GV3/20
`GV3I30
`GV1/15
`GV1I30
`50% GF
`20% GF
`30% GF
`15% GF
`30% GF
`
`Processing
`Melt Flow MF| (g/10 min) ISO 1133
`250°C / 2.16 k
`ISO 1183
`(g/cm‘)
`Density
`Moisture Absorption (%) DIN 53495
`Water Absorption
`(%) DIN 53495
`Mould Shrinkage
`(%)
`-
`Tensile Modulus
`(GPa)
`ISO 527
`UTS (or YS)
`(MPa)
`ISO 527
`Elongation
`(%)
`ISO 527
`IS Izod, 23°C
`(kJ/m’)
`ISO 180/10
`~30°C
`NIS Izod, 23°C (kJ/mz)
`~30°C
`
`ISO 180/1A
`
`,
`‘
`
`(“0)
`(°C)
`
`ISO 306
`Vicat B, 50 N
`ISO 75
`HDT, 1.8 MPa
`UL 94
`Flammability , mm
`CTE, 23l80°C (10'5/°C) DIN 53752
`DielectStr
`(kV/mm)
`IEC 243-1
`Volume Res
`($2.0m)
`IEC 93
`Surface Res
`(9)
`IEC 93
`Dielect const @ 50 Hz
`IEC 250
`@1 MHZ
`Diss Factor @ 50 Hz
`@1 MHZ
`IEC112
`(V)
`CTI
`Comments: GF = lass fibres, FL for flame retardenc .
`
`.
`
`.
`
`ISO 1325
`
`See Key to Data Sheets - Pages 139 to 142
`
`Processing
`Melt Flow MFI (9/10 min) ISO 1133
`250°C / 2.16 k
`ISO 1183
`(g/cm’)
`Density
`Moisture Absorption (%) DIN 53495
`Water Absorption
`(%) DIN 53495
`Mould Shrinkage
`(%)
`-
`Tensile Modulus
`(GPa)
`ISO 527
`UTS (or YS)
`(MPa)
`ISO 527
`Elongation
`(%)
`ISO 527
`IS Izod, 23°C
`(kJ/mz)
`ISO 180/10
`-30°C
`ISO 180/1A
`NIS Izod, 23°C (kJ/mz)
`'
`-30°C
`ISO 306
`Vicat B