`
`MINIMUM”!!!MUNIIIHIMHNIM“WNW
`
`LIBRARY OF CONG
`
`DDDDH7WH4§LU
`
`Petitioners' Exhibit 10 3, pg. 1
`
`Petitioners' Exhibit 1013, pg. 1
`
`

`

`WWmww
`mm.
`A».
`
`
`
`.$6.?er
`
`
`
`m,VJ.:..,,.,.,..,.1.s._..V,.FEEHE§§F
`
`..mXE.Sren.Dfl6P
`
`.fl.
`
`1O1
`
`3,
`
`2gD.
`
`Petitioners' Exhibit 1013, pg. 2
`
`

`

`
`
`Petitioners' Exhibit 1013, pg. 3
`
`

`

`THERMAL
`
`EXPANSION
`
`‘ Metallic Elements and Alloys
`
`Petitioners' Exhibit 1013, pg. 4
`
`

`

`THERMDPHYSICAL PROPERTIES OF MATTER
`
`The TPFIC Data Series
`
`A_ Comprehensive CompilatiOn of Data by the
`Thermophysical Properties Research Center (TPRC), Purdue University
`
`Thermal Conductivity—Metallic Elements and Alloys
`Thermal Conductivity—Nonmetallic Solids
`Thermal Conductivity—Nonmetallic Liquids and Gases
`Specific Heat—Metallic Elements and Alloys
`Specific Heat—Nonmetallic Solids
`1
`Specific Heat~Nonmetallic Liquids and Gases
`Thermal Radiative Properties—Metallic Elements and Alloys
`Thermal Radiative Properties—Nonmetallis Solids
`Volume
`Thermal Radiative Properties—Coatings
`Volume
`Thermal Diffusivity
`Volume 10.
`Volume 11. Viscosity
`Volume/12.
`Thermal Expansion—Metallic Elements and Alloys
`Volume 13.
`Thermal Expansion—Nonmetallic Solids
`
`and use its interim updating services forthe most current information.
`
`Y. S. Tauloukian, Series Editpr-
`C. Y. Ho, Series Technical Editor
`
`Vdume
`Vdume
`Vdume
`Vdume
`Vdume
`Vdume
`Vdume
`
`SOPONQPTRFDNE
`
`
`
`New data on thermophysical properties are being constantly accumulated at TPRC. Contact TPRC
`
`Petitioners' Exhibit 1013, pg. 5
`
`

`

`WT_ _
`
`“2/,
`[/4471 [cf/é ( K
`I
`(flérvvmgi‘fr-L;
`
`I
`
`A
`
`THERMDRRYEICAL RRQRERTIES or: MATTER
`VOLUME 12;)
`'
`
`"
`
`Y. S. Touluukian
`Director
`Thermophysical Properties Research Center
`and
`Distinguished Atkins Professor of Engineering
`School of Mechanical Engineering
`Purdue University
`and
`Visiting Professor of Mechanical Engineering
`Auburn University
`
`lFl/PLENUM 0 NEW YORK-WASHINGTON
`
`THERMAL _
`EXPANSION
`
`Metallic Elements and Alloys
`
`R. K .Kir-by
`Physicist
`Crystallography Section
`inorganic Materials Division
`Institute for Materials Research
`US. National Bureau of Standards
`
`Fl. E. Taylor-
`Senior Researcher
`Thermophysical Properties Research Center
`and
`Head
`Properties Research Laboratory
`School of Mechanical Engineering
`Purdue University
`
`P. D. Desai
`Assistant Senior Researcher
`Thermophysical Properties Research Center
`Purdue University
`
`Petitioners' Exhibit 1013, pg. 6
`
`

`

`Printed in the United States of America
`
`Distributed in Europe by Heyden & Son, Ltd'.
`Spectrum House, Alderton Crescent
`London NW4 3XX, England
`
`Copyright: © 1976, Purdue Research Foundation
`
`lFl/Plenum Data Company is a division of
`Plenum Publishing Corporation
`t 17th Street, New York, NY. 10011
`
`\IOHQM
`
`Library of C
`
`ongress Catalog Card Number 73-129616 (Alli)
`
`lSBN (13-Volume Set) 0—306-67020-8
`ISBN (Volume 12) 0—306—67082—1
`
`Petitioners' Exhibit 1013, pg. 7
`
`

`

`
`
`1.
`
`E LE ME NTS
`
`Figure and/or
`Table No.
`
`QOmiAwND-l
`
`GEOUPiNG OF MATERIALS AND
`
`LIST OF FIGURES AND TABLES
`
`Name
`
`Aluminum
`Antimony
`Barium
`
`9F Only provisional values calculated from density data presented.
`
`Beryllium
`Bismuth
`Cadmium
`Calcium
`Cerium
`Cesium
`Chromium
`Cobalt
`C opper
`Dysprosium
`Erbium
`Europium
`Gadolinium
`Gallium
`Germanium
`Gold
`Hafm'um
`Holmium
`Indium
`Iridium
`Iron
`- 24
`Lanthanum
`2 5
`Lead
`26
`Lithium
`27
`Lutetlum
`28
`Magnesium
`29
`Manganese
`30
`Mercury
`31
`Molybdenum
`32
`Neodymium
`33
`Nickel
`34
`Niobium
`35
`’ Osmium
`'
`36
`
`
`to +9
`H O
`
`l-‘l-‘HCOMH
`
`Hg;
`H. 01
`H C}
`H4
`HCO
`
`g: _i.
`
`NNHHow
`
`NN
`
`*
`
`* Number marked with an asterisk indicates that recommcndcd/provisional/typical values are not reported
`for this material; for others these values are reported in separate figure and table of the same number
`followed by the letter R.
`'
`'i No original—data figure given.
`
`Petitioners' Exhibit 1013, pg. 8
`
`

`

`3'7
`38
`39
`40” 1'
`41*
`42
`43
`44
`45
`4G
`47
`
`48
`49
`
`51
`52
`53
`54
`55
`56
`57
`58
`59
`60
`61
`62
`63
`64
`
`Palladium
`Platinum
`Plutonium
`Polonium
`Potassium
`Praseodymjum
`Protaotinium
`Rhenium -
`Rhodium
`Ruthenium
`Scandium
`
`Silver
`Sodium
`Strontium
`Tantalum
`Terbium
`Thallium
`Thorium
`Thulium
`Tin
`Titanium
`Tungsten
`Uranium
`Vanadium
`Ytterbium
`Yttrium
`Zinc
`Zirconium
`
`2.
`
`lNTERMETALLIC COMPOUNDS
`
`Figure and/or
`Table No.
`
`Formula
`
`6 5
`
`66A*
`6613*
`
`Ale
`
`AlzCu
`AlCu
`
`AlC u2
`66C 5*
`A14Cu9
`66M
`Aicu3
`66E *
`Al2Au
`67
`A15Fe2
`68A
`
`
`xviii Grouping of Materials and List of Figures and Tables
`
`1 .
`
`E LEMENTS (continued)
`
`Figure and/or
`Table No.
`
`'
`
`Name
`
`* Only provisional value; calculated from density data presented.
`
`* Number marked with an asterisk indicates that recommended/provisional/typical values are not reported
`for this material; for others these values are reported in separate figure and table of the same number
`followed by the letter R.
`1‘ No original—data figm'e given.
`
`Petitioners' Exhibit 1013, pg. 9
`
`

`

`
`
`Grouping of Materials and List of Figures and Tables
`
`XIX
`
`2.
`
`INTERMETALLIC COMPOUNDS (continued)
`Figure and/01'
`Table No.
`
`Formula
`
`6813
`6 8C
`6 9A
`
`6 9B
`’70
`
`’7 1
`7 2
`7 3
`’74
`7 5
`
`7 '7
`78
`
`97
`
`AlaFe
`‘ A 12 F e
`A 1 Fe
`
`AlFe3
`AIM
`
`AlNiS
`A1Ag2
`AlaU
`SbGa
`SbIn
`SbLa
`
`8-39; 7Hf2
`Being
`BemTa
`BS1 7Ta2
`B31 aU
`B01 3 Z 1‘
`Bith
`BiPt
`CdAu
`CdLi
`
`CdsMg
`CdTe
`
`CaMg2
`Celn3
`Col’da
`CeR uz
`CcSn3
`CrFe
`
`()0sz
`002 Gd
`C01 7Y2
`Co5Y
`CuaAul
`CuAu‘
`CuzMg
`
`0115an
`CuZn
`
`GdIna
`Gd7Fe“
`Gdchl3
`GaNi
`
`T No original~data figure given.
`
`4" Number marked with an asterisk indicates that recommondcd/provisional/ty‘pical values are not reported
`for this material; for others those values are reported in separate figure and table of the same number
`followed by the letter R.
`
`Petitioners' Exhibit 1013, pg. 10
`
`

`

`i No original ~da’ca figure given.
`
`
`
`Grouping of Materials and List ofFigurcs and Tables
`
`2.
`
`INTERMETALLIC COMPOUNDS (continued)
`
`Figure and/or
`Table No.
`
`Formula
`
`.
`.
`
`93* i
`99* T
`100M
`101A
`101B
`101C
`102*"r
`103
`104M
`105*1‘
`106
`107
`108A
`108B
`109A
`10913
`110
`111*1‘
`112*T
`113
`114A
`1111B
`115* T
`116
`117
`118* T
`119*“r
`120* ’r
`
`121* ‘r
`122*?
`
`123“
`24’“
`' 25
`I
`126
`’ 27A
`2713
`128A
`28B
`129
`130a”
`' 31
`' 32
`
`33
`34*”r
`
`-
`
`GaAg3
`GeLa
`GeMg2
`GezPr
`GePr
`GeaPr5
`AuAMn
`AugMn
`AuMn
`Au4V
`AuZn
`Hoan
`[rian
`InsPr
`InsYb
`In3Y
`FE17L112
`FeNi3
`FeRh
`F91 7Y2
`LaRu2
`LaSna
`PbLi
`MgAg
`MgZSn
`Man
`MnNi
`MnPd
`
`MnaPt
`MnPt
`
`111ng
`NiTi
`Ni5Y
`NbSSn
`Pdasn
`PdsYb
`PrRu2
`PrSn3
`SmAg3
`Agar 1b
`Aan
`Na’l‘l
`
`Y17Zn2
`ZnZZr
`
`* Number marked with an asterisk indicates that recommended/provisional/typical values are not reported
`for this material; for others these values are reported in separate figure and table of the same number
`followed by the letter R .
`
`Petitioners' Exhibit 1013, pg. 11
`
`

`

`xxii
`
`Grouping of Materials and List of Figures and Tables
`
`3. BINARY ALLOY SYSTEMS (continued)
`Figure and/or
`,
`Table No.
`
`Name
`
`'
`
`1640*
`165*1‘
`166* T
`167* T
`168
`169* ’F
`170*1'
`171* 1‘
`172A*
`172134? T
`172C
`173
`174A*
`174B
`17 5A
`17 5B
`17G
`1 77
`178*
`179*
`180
`181
`182* T
`183
`184M
`184B
`185
`186* T
`187A“
`1873 *
`1870*
`18 713*
`188%
`189a6 T
`190
`191*
`192
`193
`194
`195* 1“
`196A*
`196B
`
`T No original—data. figure given.
`
`C obalt-Palladium
`Cobalt—Platinum
`Cobalt—Tantalum
`Cobalt—’l'itanmm
`Cobalt—Tungsten
`Cobalt~Vanadium
`Cobalt—Zirconium
`Copper—Gold
`Copper-Indium
`Coppexwlfon
`Copper~Magneslum
`Copper—Manganese
`Copper —Molybdcnum
`Copper—Nickel
`Copper—Tin
`Copper ~Tungsten
`Copper—Zinc
`Dysprosium~Ta11ta1un1
`Gallium-Plutonium
`Gold—Indium
`Gold—Palladimn
`Gold ~I’latinum
`Gold—Silver
`Hafnium—Zirconium
`Indium—Lead
`Indium—Silver
`Indium—Thallium
`Indium—Tin
`Iridium-Osmium
`- Ifidium—Hatinum
`lrldiun1~Rllemum
`fridlum~Rhodium
`Iron—Manganese
`lion—Molybdenum
`Iron~Vlckel
`Iron—Platinum
`Iron—R hodium
`Iron—Silicon
`Lead~Tin
`Lead-Thallium
`Magne sium—Manganese
`Magnesium-Nickel
`
`.
`
`Formula
`
`c o—Pd
`Co—P’c
`Co—Ta
`Co~Ti
`Co—W
`Co—v
`Co—Zr
`Cu—Au
`Cu~In
`Cu~Fe
`Cu—Mg
`Cu~Mn
`Cu—Mo
`Cu—Ni
`Cu-Sn
`Cu—W
`Cu—Zn
`7 Dy~Ta
`Ga ~Pu
`Au~1n
`Au—Pd
`Au—Pt
`Au-Ag'
`Hf—Zr
`In—Pb
`In—Ag
`In—Tl
`In—Sn
`Ir -OS
`Ir—Pt
`Ir—Re
`Ir—Rh
`Fe—Mn
`Fe—Mo
`Fe—Ni
`Fe-Pt
`Fe—Rh
`Fe—Si
`Pb-Sn
`l’b—Tl
`Mg~Mn
`Mg~Ni
`
`1“ Number marked with an asterisk indicates that recommended/provis1onal/typical values are not reported
`for this material; for others these values are reported in separate figure and table of the same number
`followed by the letter R.
`
`Petitioners' Exhibit 1013, pg. 12
`
`

`

`3.
`
`BINARY ALLOY SYSTEMS (continued)
`
`Figure and/or
`Table No.
`
`Name
`
`1 9’7
`198
`1 99A"
`199B
`200A
`20 013*
`2000*
`201* 7‘
`202
`203
`204A"
`20 413*
`20 5
`20 6
`207
`208
`209
`210*
`211
`212
`213
`214
`215
`216
`
`Magne sium—Sllver
`Magnesium—Tin
`Magnesium~Uranium
`Magne sium—Zinp
`Manganese—Nickel
`Manganese—Silver
`Manganese~Titanium
`Molybdenum~Nickel
`Molybdenum—Niobium
`Molybdenum—Rhean
`.Molybdenum—Selenium
`Molybdenum—T ellurium '
`Molybdenum-Titanium
`Molybdenum—Tungsten
`Molybd enum—Uranium
`Molybdenum~Vanadium
`Nickel—Palladium
`Nickel—Platinum
`Nickel—Silicon
`Nickel—Tin
`Nickel—’l‘itanium
`Nickel—Tungsten
`Nickel—Vanadium
`Nickel—Zinc
`
`I
`
`* Number marked with an asterisk indicates that recmhmended/provisional/typical values are not reported
`for this material; for others these values are reported in separate IigLu'e and table of the same number
`followed by the letter R.
`
`Grouping of Materials and List of Figures and Tables
`
`xxiii
`
`‘
`
`Formula
`
`Mg—Ag
`Mg-Sn
`Mg—U
`Mg—Zn
`Mn—Ni
`Mn~Ag
`Mn—Ti
`Mo—Ni
`MO ~Nb
`Mo—R 8
`Mo—Se
`MomTe
`M0~Ti
`Mo~W
`Mo—U
`Mo—V
`Ni—Pd
`Ni—Pt
`Ni—Si
`Ni—Sn '
`Ni—Ti
`Ni—W
`Ni—V
`
`Nb —Re
`- Nb~Ta
`Nb—U
`Nb—V
`Nb—Zr
`Pd~Ag
`Pt-Rh
`Pt~Ru
`Ber-W
`Ag—Sn
`Tavw
`Tb —Y
`Sn—Zr
`Ti—W
`Ti—V
`Ti—z r
`U— Zr
`
`I 1' No original—data figure-given.
`
`Niobium—Rhenium
`217A
`Niobium—Tantalum
`217B
`Niobium—Uranium
`218A
`7 Niobium—Vanadium
`218B”
`Niobium—Zirconium
`21 9
`Palladium—Silver
`220
`Platinum—Rhodium
`221*
`Platinum—Ruthenium
`222
`Rhenium—Tungsten
`223
`Silver ~Tin
`224
`Tantalum—Tungsten ,
`225
`Terbium—Yttrium
`22 6”"
`Tin—Zirconium
`227*
`'l‘itaiiium~'£ungsten
`228* T
`Titanium-Vanadium
`229
`Titanium—Zirconiiim
`230
`*
`Uranium—Zirconium
`231
`
`
`Petitioners' Exhibit 1013, pg. 13
`
`

`

`xxiv
`
`Grouping of Materials and List of Figures and Tables
`
`4. MULTIPLE ALLOYS
`
`Figure and/or
`Table No.
`
`Name
`
`Formula
`
`T No original—data figure given.
`
`Al + Be + 2X1
`Aluminum + Beryllium + EXj
`A1+ Cu + Exi
`Aluminum + Copper + 2X1
`A1 + Fe + 2X1
`Aluminum + Iron + 73Xi
`Al + Mg + ZXj
`Aluminum + Magnesium + 22Xi
`Al +. Mn + 23Xj
`Aluminum + Manganese + EXj
`A1+ Ni + Exi
`Aluminum + Nickel + EXi
`Al + Si + 2X1
`Aluminum + Silicon + ZXi
`A1+ Zn+ EXi
`Aluminum + Zinc + ZXi _
`Be + A1 + ‘EXi
`Beryllium + Aluminum + EXi
`Cr + Fe + EXi
`Chromium + Iron + EXi
`Cr + Si + 2X1
`Chromium + Silicon+ 2X1
`Co + Cr + EXi
`Cobalt + Chromium + EXi
`Co + Fe + 2X1
`Cobalt + Iron + 2X1
`Co + Ni + ZXi
`Cobalt + Nickel + EXi
`Cu + Al + Exi
`Copper + Aluminum + Exi
`Cu + Be 4- EXi
`Copper + Beryllium+ 23Xi
`Cu + Pb + ZXi
`Copper + Lead + EXi
`Cu + Mn + ZXi
`Copper + Manganese + EXi
`Cu + Ni 4- 22Xi
`Copper + Nickel + )SXi
`Cu+ Si + EXi
`Copper + Silicon+ 2X1
`Cu + Sn+ EXi
`Copper + Tin+ EXi
`'
`Cu + Zn + Exi
`Co‘pper + Zinc + 2X1
`Dy + Ta + EXi
`Dysprosium + Tantalum + 23Xi
`Au + Ag + zxi
`Gold + Silver + zxi
`Ir + Os + ZXi
`Iridium + Osmium + 2X1
`Ir + Pt + EXi
`Iridium + Platinum + ZIXi
`11' + Re + EXi
`Iridium + Rhenjum + EXi
`Ir + Rh + zxi
`Iridium + Rhodium + ZXi
`Fe + C + 2X1
`Iron+ Carbon+ EXi
`Fe + 01- + ZXi
`Iron ~x~ Chromium + EXi
`Fe + Co + EXi
`Iron + Cobalt + EX].
`Fe 4- Cu + 23Xi
`Iron+ Copper + EXi
`Fe + Mn + Exi-
`Iron + Manganese + 2X1
`Fe + Ni + EXi
`Iron+ Nicke1-+ ZXi
`Fe + W + EXi
`Iron + Tungsten + 22Xi
`Mg + Al + EXi
`Magnesium + Aluminum + 23Xi
`Mg + Cu + EXi
`Magnesium + Copper + EX1
`Mg + Th + EXi
`Magnesium + Thorium + EXi
`Mg + Zn + 2X1
`Magnesium + Zinc + EXi
`M0 + Ti + zxi
`Molybdenum + Titanium+ 2x1
`Ni + Al + zxi
`Nickel + Aluminum + Exi
`Ni + Cr + EXi
`. Nickel + Chromium+ 23Xi
`
`Nickel + Cobalt + EXi Ni + Co + EXi
`
`232
`233
`234*
`235
`236
`237
`238
`239
`240
`241
`242
`243
`244
`245
`246
`247
`248
`249*”
`250
`251
`252
`_
`253
`254')” ‘
`255*"
`256A
`256B
`256C
`256D
`‘ 257
`258
`259
`260
`261
`262
`263
`264
`265A
`265B
`265C
`266M
`267* l
`268
`269
`
`-
`
`* Number marked with an asterisk indicates that recommended/pr0visional/typical values are not reported
`for this material; for others these values are reported in separate figure and table of the same number
`followed by the letter R.
`
`Petitioners' Exhibit 1013, pg. 14
`
`

`

`Name
`
`Figure and/or
`Table No.
`270
`271*
`272
`273
`
`274* 1‘
`275
`276
`277*
`278
`279* i
`280A
`280B
`281
`282
`283A
`283B
`284
`285* T
`286A*
`2863*
`287*"
`288*
`289* T
`290* T
`291M
`292‘“
`293*
`
`
`
`* Number marked with an asterisk indicates that recommended/provisionai/typical values are not reported
`7 for this material; for others these values are reported in separate figure and table of the same number
`followed by the letter R .
`T No original—data figure given.
`
`Grouping ofMater'z'als and List of Figures and Tables
`
`4. MULTIPLE ALLOYS (continued)
`
`Formula
`
`’Ni+ Cu+ 2X1
`Ni+Fe+ EXi
`Ni+ Mn+ 2X1
`Nil Mo+ EXi
`Ni+ Si+ EXi
`Nb+ Mo+ Exi
`Nb+ Ta+2Xi
`Nb+ Ti+ {)Xi
`Nb-i- W+ EXi
`Pd'i‘Au‘i‘in
`Ta+Nb+ZIXi
`Ta+W+ XXi
`Ti + Al+ 2X1
`Ti+ Cr+ 2X.1
`Ti+ Sn+ 2X1
`Ti+V+ 22Xi
`W+ Ni+23Xi
`W+Re+ 2Xi
`U+Al+ 23Xi
`U+ M0+ ZXi
`U‘I-Nb+ EXi
`U+ Pu+ 2X1
`U+V+ EXi'
`V+ Cr+ EXi
`V+ Ti+ZJXi
`Zr+ Sn+ 2X1
`Zr+ Ti+EX‘i
`
`.
`
`Nickel + Copper + ZXi
`Nickel + Iron + 2Xi
`Nickel + Manganese + ZXi
`Nickel + Molybdenum + 2X1
`Nickel + Silicon 7| EXi
`Niobium + Molybdenum + EXi
`Niobium + Tantalum + EXi
`Niobium + Titanium + 2X1
`Niobium + Tungsten + ZXi
`Palladium + Gold + EXi
`Tantalum »| Niobium + Exi
`Tantalum + Tungsten + 2X1
`Titanium + Aluminum + 2X1
`Titanium + Chromium + 2X1
`Titanium + Tin + zxi
`Titanium + Vanadium + 2X1
`Tungsten + Nickel + 2X1
`Tungsten + Rhenium + EXi
`Uranium + Aluminum + EXi
`Uranium + Molybdenum + 2Xi
`Uranium + Niobium + 2X1
`Uranium ‘l' Plutonium + EXi
`Uranium + Vanadium + 2X1
`Vanadium + Chromium + EXi
`Vanadium + Titanium + ZXi
`Zirconium + Tin+ 23Xi
`Zirconium + Titanium + ZXi
`
`XXV
`
`Petitioners' Exhibit 1013, pg. 15
`
`

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`1. ELEMENTS
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`Numerical Data on Thermal Linear Expansion of
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`Petitioners' Exhibit 1013, pg. 16
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`Petitioners' Exhibit 1013, pg. 17
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`Petitioners' Exhibit 1013, pg. 18
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`Petitioners' Exhibit 1013, pg. 19
`
`

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`Petitioners' Exhibit 1013, pg. 20
`
`

`

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`Petitioners' Exhibit 1013, pg. 21
`
`

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`Petitioners' Exhibit 1013, pg. 24
`
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