throbber
1.57
`1.58
`1.58
`1.59
`1.59
`1.60
`2.11
`2.13
`2.13
`2.14
`2.26
`2.45
`2.50
`2.50
`2.50
`3.36
`
`4.28
`4.30
`4.62
`4.64
`
`7.07
`7.07
`7.08
`7.08
`7.09
`7.09
`7.11
`7.11
`7.11
`7.11
`7.23
`7.23
`7.24
`7.25
`7.25
`7.26
`7.27
`7.28
`7.28
`7.29
`7.29
`7.29
`7.36
`7.38
`7.38
`7.39
`7.40
`7.41
`8.17
`
`12.51
`
`
`
`2007KEYS.731C
`13-112-HND110
`DMSO, H-1
`NUMEGA 10-23-2020
`
`2.00
`
`1.06
`2.97
`2.93
`
`0.73
`
`1.01
`
`1.00
`
`0.96
`1.00
`0.99
`1.00
`
`0.98
`
`0.93
`
`13.0
`
`12.5
`
`12.0
`
`11.5
`
`11.0
`
`10.5
`
`10.0
`
`9.5
`
`9.0
`
`8.5
`
`8.0
`
`7.5
`
`7.0
`
`6.5
`6.0
`f1 (ppm)
`
`5.5
`
`5.0
`
`4.5
`
`4.0
`
`3.5
`
`3.0
`
`2.5
`
`2.0
`
`1.5
`
`1.0
`
`0.5
`
`0.0
`
`-0.5
`
`Page 1 of 31
`
`EISAI EXHIBIT 1014
`
`

`

`12.51
`
`0.93
`
`
`
`2007KEYS.731C
`13-112-HND110
`DMSO, H-1
`NUMEGA 10-23-2020
`
`12.8
`
`12.7
`
`12.6
`
`12.5
`
`12.4
`
`12.3
`
`12.2
`f1 (ppm)
`
`12.1
`
`12.0
`
`11.9
`
`11.8
`
`11.7
`
`11.6
`
`11.5
`
`Page 2 of 31
`
`

`

`7.07
`7.07
`7.08
`7.08
`7.09
`7.09
`7.11
`7.11
`7.11
`7.11
`7.23
`7.23
`7.24
`7.25
`7.25
`7.26
`7.27
`7.28
`7.28
`7.29
`7.29
`7.29
`7.36
`7.38
`7.38
`7.39
`7.40
`7.41
`
`8.17
`
`
`
`2007KEYS.731C
`13-112-HND110
`DMSO, H-1
`NUMEGA 10-23-2020
`
`0.96
`
`1.00
`
`0.99
`
`1.00
`
`0.98
`
`8.5
`
`8.4
`
`8.3
`
`8.2
`
`8.1
`
`8.0
`
`7.9
`
`7.8
`
`7.7
`
`7.6
`
`7.5
`
`7.4
`f1 (ppm)
`
`7.3
`
`7.2
`
`7.1
`
`7.0
`
`6.9
`
`6.8
`
`6.7
`
`6.6
`
`6.5
`
`6.4
`
`6.3
`
`Page 3 of 31
`
`

`

`1.57
`1.58
`1.58
`1.59
`1.59
`1.60
`
`2.11
`2.13
`2.13
`2.14
`2.26
`
`2.45
`2.50
`2.50
`2.50
`
`3.36
`
`4.28
`4.30
`
`4.62
`4.64
`
`
`
`2007KEYS.731C
`13-112-HND110
`DMSO, H-1
`NUMEGA 10-23-2020
`
`2.00
`
`1.06
`
`2.97
`
`2.93
`
`0.73
`
`1.01
`
`1.00
`
`4.8
`
`4.7
`
`4.6
`
`4.5
`
`4.4
`
`4.3
`
`4.2
`
`4.1
`
`4.0
`
`3.9
`
`3.8
`
`3.7
`
`3.6
`
`3.5
`
`3.4
`
`3.3
`
`3.2
`3.1
`3.0
`f1 (ppm)
`
`2.9
`
`2.8
`
`2.7
`
`2.6
`
`2.5
`
`2.4
`
`2.3
`
`2.2
`
`2.1
`
`2.0
`
`1.9
`
`1.8
`
`1.7
`
`1.6
`
`1.5
`
`1.4
`
`Page 4 of 31
`
`

`

`2.49
`2.50
`2.50
`2.50
`2.51
`
`3.33
`
`5.82
`6.43
`6.43
`6.44
`6.44
`6.45
`6.45
`6.45
`6.45
`
`7.29
`7.29
`7.30
`7.31
`7.32
`7.33
`7.84
`7.84
`
`
`
`2007KEYS.731D
`13-112-HND300
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.54
`
`2.25
`
`1.10
`
`1.06
`
`1.00
`
`10.0
`
`9.5
`
`9.0
`
`8.5
`
`8.0
`
`7.5
`
`7.0
`
`6.5
`
`6.0
`
`5.5
`
`5.0
`4.5
`f1 (ppm)
`
`4.0
`
`3.5
`
`3.0
`
`2.5
`
`2.0
`
`1.5
`
`1.0
`
`0.5
`
`0.0
`
`-0.5
`
`Page 5 of 31
`
`

`

`5.82
`
`6.43
`6.43
`6.44
`6.44
`6.45
`6.45
`6.45
`6.45
`
`7.29
`7.29
`7.30
`7.31
`7.32
`7.33
`
`7.84
`7.84
`
`
`
`2007KEYS.731D
`13-112-HND300
`DMSO, H-1
`NUMEGA 10-23-2020
`
`2.25
`
`1.10
`
`1.06
`
`1.00
`
`8.2
`
`8.1
`
`8.0
`
`7.9
`
`7.8
`
`7.7
`
`7.6
`
`7.5
`
`7.4
`
`7.3
`
`7.2
`
`7.1
`
`7.0
`6.9
`f1 (ppm)
`
`6.8
`
`6.7
`
`6.6
`
`6.5
`
`6.4
`
`6.3
`
`6.2
`
`6.1
`
`6.0
`
`5.9
`
`5.8
`
`5.7
`
`5.6
`
`Page 6 of 31
`
`

`

`2.49
`2.50
`2.50
`2.50
`2.51
`
`3.33
`
`
`
`2007KEYS.731D
`13-112-HND300
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.54
`
`3.6
`
`3.5
`
`3.4
`
`3.3
`
`3.2
`
`3.1
`
`3.0
`
`2.9
`f1 (ppm)
`
`2.8
`
`2.7
`
`2.6
`
`2.5
`
`2.4
`
`2.3
`
`2.2
`
`Page 7 of 31
`
`

`

`1.48
`1.49
`1.50
`1.51
`1.69
`1.70
`1.70
`1.71
`2.03
`2.38
`2.49
`2.50
`2.50
`2.50
`2.51
`2.62
`2.63
`2.63
`2.65
`3.33
`
`4.28
`4.30
`4.66
`4.68
`7.08
`7.09
`7.09
`7.10
`7.10
`7.10
`7.11
`7.11
`7.12
`7.12
`7.38
`7.39
`7.39
`7.40
`7.40
`7.41
`7.43
`7.43
`7.43
`7.44
`7.45
`7.46
`7.46
`7.61
`7.62
`7.63
`7.63
`7.64
`7.65
`7.88
`7.89
`7.90
`7.91
`8.12
`8.31
`8.32
`
`11.21
`
`
`
`2007KEYS.731A
`13-113-2X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.04
`1.03
`
`3.03
`3.04
`1.03
`
`2.61
`
`1.03
`
`1.03
`
`1.00
`3.08
`1.01
`1.00
`1.02
`0.96
`
`0.99
`
`12.0
`
`11.5
`
`11.0
`
`10.5
`
`10.0
`
`9.5
`
`9.0
`
`8.5
`
`8.0
`
`7.5
`
`7.0
`
`6.5
`
`6.0
`5.5
`f1 (ppm)
`
`5.0
`
`4.5
`
`4.0
`
`3.5
`
`3.0
`
`2.5
`
`2.0
`
`1.5
`
`1.0
`
`0.5
`
`0.0
`
`-0.5
`
`Page 8 of 31
`
`

`

`11.21
`
`0.99
`
`
`
`2007KEYS.731A
`13-113-2X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`11.8
`
`11.7
`
`11.6
`
`11.5
`
`11.4
`
`11.3
`
`11.2
`
`11.1
`
`11.0
`
`10.9
`
`10.8
`f1 (ppm)
`
`10.7
`
`10.6
`
`10.5
`
`10.4
`
`10.3
`
`10.2
`
`10.1
`
`10.0
`
`9.9
`
`9.8
`
`Page 9 of 31
`
`

`

`7.08
`7.09
`7.09
`7.10
`7.10
`7.10
`7.11
`7.11
`7.12
`7.12
`7.38
`7.39
`7.39
`7.40
`7.40
`7.41
`7.43
`7.43
`7.43
`7.44
`7.45
`7.46
`7.46
`7.61
`7.62
`7.63
`7.63
`7.64
`7.65
`
`7.88
`7.89
`7.90
`7.91
`
`8.12
`
`8.31
`8.32
`
`
`
`2007KEYS.731A
`13-113-2X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.00
`
`3.08
`
`1.01
`
`1.00
`
`1.02
`
`0.96
`
`8.9
`
`8.8
`
`8.7
`
`8.6
`
`8.5
`
`8.4
`
`8.3
`
`8.2
`
`8.1
`
`8.0
`
`7.9
`
`7.8
`
`7.7
`7.6
`f1 (ppm)
`
`7.5
`
`7.4
`
`7.3
`
`7.2
`
`7.1
`
`7.0
`
`6.9
`
`6.8
`
`6.7
`
`6.6
`
`6.5
`
`6.4
`
`Page 10 of 31
`
`

`

`1.48
`1.49
`1.50
`1.51
`1.69
`1.70
`1.70
`1.71
`
`2.03
`
`2.38
`2.49
`2.50
`2.50
`2.50
`2.51
`2.62
`2.63
`2.63
`2.65
`
`3.33
`
`4.28
`4.30
`
`4.66
`4.68
`
`
`
`2007KEYS.731A
`13-113-2X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.04
`
`1.03
`
`3.03
`
`3.04
`
`1.03
`
`2.61
`
`1.03
`
`1.03
`
`4.9
`
`4.8
`
`4.7
`
`4.6
`
`4.5
`
`4.4
`
`4.3
`
`4.2
`
`4.1
`
`4.0
`
`3.9
`
`3.8
`
`3.7
`
`3.6
`
`3.5
`
`3.4
`
`3.3
`
`3.2
`3.1
`f1 (ppm)
`
`3.0
`
`2.9
`
`2.8
`
`2.7
`
`2.6
`
`2.5
`
`2.4
`
`2.3
`
`2.2
`
`2.1
`
`2.0
`
`1.9
`
`1.8
`
`1.7
`
`1.6
`
`1.5
`
`1.4
`
`Page 11 of 31
`
`

`

`1.48
`1.49
`1.50
`1.51
`1.69
`1.70
`1.71
`1.72
`2.03
`2.38
`2.49
`2.50
`2.50
`2.50
`2.51
`2.62
`2.63
`2.64
`2.65
`3.33
`
`4.28
`4.31
`4.66
`4.68
`7.08
`7.09
`7.09
`7.10
`7.10
`7.10
`7.11
`7.11
`7.12
`7.12
`7.38
`7.39
`7.39
`7.40
`7.40
`7.41
`7.43
`7.43
`7.43
`7.44
`7.45
`7.46
`7.46
`7.61
`7.62
`7.63
`7.63
`7.64
`7.65
`7.88
`7.89
`7.90
`7.91
`8.12
`8.31
`8.32
`
`11.21
`
`
`
`2007KEYS.731B
`13-115-1X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.07
`1.08
`3.17
`
`3.17
`
`1.09
`
`2.20
`
`1.08
`
`1.08
`
`1.04
`2.05
`1.16
`1.06
`1.03
`1.06
`1.00
`
`0.97
`
`12.0
`
`11.5
`
`11.0
`
`10.5
`
`10.0
`
`9.5
`
`9.0
`
`8.5
`
`8.0
`
`7.5
`
`7.0
`
`6.5
`
`6.0
`5.5
`f1 (ppm)
`
`5.0
`
`4.5
`
`4.0
`
`3.5
`
`3.0
`
`2.5
`
`2.0
`
`1.5
`
`1.0
`
`0.5
`
`0.0
`
`-0.5
`
`Page 12 of 31
`
`

`

`11.21
`
`0.97
`
`
`
`2007KEYS.731B
`13-115-1X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`11.9
`
`11.8
`
`11.7
`
`11.6
`
`11.5
`
`11.4
`
`11.3
`
`11.2
`
`11.1
`11.0
`f1 (ppm)
`
`10.9
`
`10.8
`
`10.7
`
`10.6
`
`10.5
`
`10.4
`
`10.3
`
`10.2
`
`Page 13 of 31
`
`

`

`7.08
`7.09
`7.09
`7.10
`7.10
`7.10
`7.11
`7.11
`7.12
`7.12
`7.38
`7.39
`7.39
`7.40
`7.40
`7.41
`7.43
`7.43
`7.43
`7.44
`7.45
`7.46
`7.46
`7.61
`7.62
`7.63
`7.63
`7.64
`7.65
`
`7.88
`7.89
`7.90
`7.91
`
`8.12
`
`8.31
`8.32
`
`
`
`2007KEYS.731B
`13-115-1X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.04
`
`2.05
`
`1.16
`
`1.06
`
`1.03
`
`1.06
`
`1.00
`
`8.8
`
`8.7
`
`8.6
`
`8.5
`
`8.4
`
`8.3
`
`8.2
`
`8.1
`
`8.0
`
`7.9
`
`7.8
`
`7.7
`f1 (ppm)
`
`7.6
`
`7.5
`
`7.4
`
`7.3
`
`7.2
`
`7.1
`
`7.0
`
`6.9
`
`6.8
`
`6.7
`
`6.6
`
`Page 14 of 31
`
`

`

`1.48
`1.49
`1.50
`1.51
`1.69
`1.70
`1.71
`1.72
`
`2.03
`
`2.38
`2.49
`2.50
`2.50
`2.50
`2.51
`2.62
`2.63
`2.64
`2.65
`
`3.33
`
`4.28
`4.31
`
`4.66
`4.68
`
`
`
`2007KEYS.731B
`13-115-1X
`DMSO, H-1
`NUMEGA 10-23-2020
`
`1.07
`
`1.08
`
`3.17
`
`3.17
`
`1.09
`
`2.20
`
`1.08
`
`1.08
`
`4.8
`
`4.7
`
`4.6
`
`4.5
`
`4.4
`
`4.3
`
`4.2
`
`4.1
`
`4.0
`
`3.9
`
`3.8
`
`3.7
`
`3.6
`
`3.5
`
`3.4
`
`3.3
`
`3.2
`3.1
`f1 (ppm)
`
`3.0
`
`2.9
`
`2.8
`
`2.7
`
`2.6
`
`2.5
`
`2.4
`
`2.3
`
`2.2
`
`2.1
`
`2.0
`
`1.9
`
`1.8
`
`1.7
`
`1.6
`
`1.5
`
`Page 15 of 31
`
`

`

`18.23
`19.28
`24.48
`26.01
`
`33.45
`39.01
`39.18
`39.34
`39.51
`39.68
`39.84
`40.01
`
`70.68
`
`113.79
`113.96
`115.06
`115.23
`
`124.33
`124.35
`130.24
`130.31
`
`139.11
`
`144.68
`144.74
`148.99
`
`155.79
`158.63
`161.07
`163.01
`
`172.25
`
`
`
`2007KEYS.731G
`13-112-HND110
`DMSO, C-13
`NUMEGA 10-23-2020
`
`200
`
`190
`
`180
`
`170
`
`160
`
`150
`
`140
`
`130
`
`120
`
`110
`
`100
`f1 (ppm)
`
`90
`
`80
`
`70
`
`60
`
`50
`
`40
`
`30
`
`20
`
`10
`
`0
`
`Page 16 of 31
`
`

`

`113.79
`113.96
`115.06
`115.23
`
`124.33
`124.35
`
`130.24
`130.31
`
`139.11
`
`144.68
`144.74
`
`148.99
`
`155.79
`
`158.63
`
`161.07
`
`163.01
`
`172.25
`
`
`
`2007KEYS.731G
`13-112-HND110
`DMSO, C-13
`NUMEGA 10-23-2020
`
`175
`
`170
`
`165
`
`160
`
`155
`
`150
`
`145
`f1 (ppm)
`
`140
`
`135
`
`130
`
`125
`
`120
`
`115
`
`110
`
`Page 17 of 31
`
`

`

`18.23
`19.28
`
`24.48
`
`26.01
`
`33.45
`
`39.01
`39.18
`39.34
`39.51
`39.68
`39.84
`40.01
`
`70.68
`
`
`
`2007KEYS.731G
`13-112-HND110
`DMSO, C-13
`NUMEGA 10-23-2020
`
`80
`
`75
`
`70
`
`65
`
`60
`
`55
`
`50
`
`45
`f1 (ppm)
`
`40
`
`35
`
`30
`
`25
`
`20
`
`15
`
`Page 18 of 31
`
`

`

`17.80
`18.40
`
`24.40
`26.92
`34.11
`39.01
`39.18
`39.34
`39.51
`39.68
`39.84
`40.01
`
`70.81
`
`113.66
`113.83
`114.23
`115.66
`115.83
`124.74
`125.02
`125.17
`130.07
`130.14
`135.10
`135.29
`139.37
`145.00
`145.06
`148.55
`148.93
`154.43
`155.53
`156.40
`158.49
`161.04
`162.98
`168.72
`
`
`
`2007KEYS.731E
`13-113-2X
`DMSO, C-13
`NUMEGA 10-23-2020
`
`200
`
`190
`
`180
`
`170
`
`160
`
`150
`
`140
`
`130
`
`120
`
`110
`
`100
`f1 (ppm)
`
`90
`
`80
`
`70
`
`60
`
`50
`
`40
`
`30
`
`20
`
`10
`
`Page 19 of 31
`
`

`

`113.66
`113.83
`114.23
`115.66
`115.83
`
`124.74
`125.02
`125.17
`
`130.07
`130.14
`
`135.10
`135.29
`
`139.37
`
`145.00
`145.06
`
`148.55
`148.93
`
`154.43
`155.53
`156.40
`
`158.49
`
`161.04
`
`162.98
`
`168.72
`
`
`
`2007KEYS.731E
`13-113-2X
`DMSO, C-13
`NUMEGA 10-23-2020
`
`170
`
`165
`
`160
`
`155
`
`150
`
`145
`
`140
`f1 (ppm)
`
`135
`
`130
`
`125
`
`120
`
`115
`
`110
`
`Page 20 of 31
`
`

`

`17.80
`18.40
`
`24.40
`
`26.92
`
`34.11
`
`39.01
`39.18
`39.34
`39.51
`39.68
`39.84
`40.01
`
`70.81
`
`
`
`2007KEYS.731E
`13-113-2X
`DMSO, C-13
`NUMEGA 10-23-2020
`
`80
`
`75
`
`70
`
`65
`
`60
`
`55
`
`50
`
`45
`f1 (ppm)
`
`40
`
`35
`
`30
`
`25
`
`20
`
`15
`
`Page 21 of 31
`
`

`

`17.80
`18.40
`
`24.40
`26.91
`34.10
`39.01
`39.18
`39.34
`39.51
`39.68
`39.84
`40.01
`
`70.81
`
`113.66
`113.82
`114.23
`115.66
`115.83
`124.74
`125.01
`125.17
`130.07
`130.13
`135.09
`135.29
`139.37
`145.00
`145.06
`148.55
`148.93
`154.43
`155.53
`156.40
`158.49
`161.04
`162.97
`168.72
`
`
`
`2007KEYS.731F
`13-115-1X
`DMSO, C-13
`NUMEGA 10-23-2020
`
`200
`
`190
`
`180
`
`170
`
`160
`
`150
`
`140
`
`130
`
`120
`
`110
`
`100
`f1 (ppm)
`
`90
`
`80
`
`70
`
`60
`
`50
`
`40
`
`30
`
`20
`
`10
`
`0
`
`Page 22 of 31
`
`

`

`113.66
`113.82
`114.23
`115.66
`115.83
`
`124.74
`125.01
`125.17
`
`130.07
`130.13
`
`135.09
`135.29
`
`139.37
`
`145.00
`145.06
`
`148.55
`148.93
`
`154.43
`155.53
`156.40
`
`158.49
`
`161.04
`
`162.97
`
`168.72
`
`
`
`2007KEYS.731F
`13-115-1X
`DMSO, C-13
`NUMEGA 10-23-2020
`
`170
`
`165
`
`160
`
`155
`
`150
`
`145
`
`140
`f1 (ppm)
`
`135
`
`130
`
`125
`
`120
`
`115
`
`110
`
`Page 23 of 31
`
`

`

`17.80
`18.40
`
`24.40
`
`26.91
`
`34.10
`
`39.01
`39.18
`39.34
`39.51
`39.68
`39.84
`40.01
`
`70.81
`
`
`
`2007KEYS.731F
`13-115-1X
`DMSO, C-13
`NUMEGA 10-23-2020
`
`75
`
`70
`
`65
`
`60
`
`55
`
`50
`
`45
`f1 (ppm)
`
`40
`
`35
`
`30
`
`25
`
`20
`
`15
`
`Page 24 of 31
`
`

`

` NuMega Resonance Labs
` Sample Name: 13-112-HND110 2007KEYS.731D
` Acq. Date: Thursday, October 22,
` 2020
` +Q1: 12 MCA scans from Sample 34 (13-112-HND110 2007KEYS.731D) of 20...
`
` Polarity/Scan Type: Positive Q1 MS
`
`Max. 7.7e6 cps.
`
`317.1
`
`250
`
`300
`
`350
`
`400
`
`450
`m/z, Da
`
`500
`
`550
`
`600
`
`650
`
`700
`
`7.6e6
`
`7.4e6
`
`7.2e6
`
`7.0e6
`
`6.8e6
`
`6.6e6
`
`6.4e6
`
`6.2e6
`
`6.0e6
`
`5.8e6
`
`5.6e6
`
`5.4e6
`
`5.2e6
`
`5.0e6
`200
`
`Intensity, cps
`
`Page 25 of 31
`
`

`

` Polarity/Scan Type: Negative Q1 MS
`
`Max. 2.4e7 cps.
`
`631.1
`
` NuMega Resonance Labs
` Sample Name: 13-112-HND110 2007KEYS.731D
` Acq. Date: Thursday, October 22,
` 2020
` -Q1: 12 MCA scans from Sample 35 (13-112-HND110 2007KEYS.731D) of 201...
`
`315.0
`
`2.4e7
`
`2.3e7
`
`2.2e7
`
`2.1e7
`
`2.0e7
`
`1.9e7
`
`1.8e7
`
`1.7e7
`
`1.6e7
`
`1.5e7
`
`1.4e7
`
`1.3e7
`
`1.2e7
`
`1.1e7
`
`1.0e7
`
`Intensity, cps
`
`200
`
`250
`
`300
`
`350
`
`400
`
`450
`m/z, Da
`
`500
`
`550
`
`600
`
`650
`
`700
`
`Page 26 of 31
`
`

`

` NuMega Resonance Labs
` Sample Name: 13-113-2X 2007KEYS.731A
` Acq. Date: Thursday, October 22,
` 2020
` +Q1: 12 MCA scans from Sample 27 (13-113-2X 2007KEYS.731A) of 2010KEY...
`
` Polarity/Scan Type: Positive Q1 MS
`
`Max. 8.0e5 cps.
`
`433.1
`
`8.00e5
`
`7.95e5
`
`7.90e5
`
`7.85e5
`
`7.80e5
`
`7.75e5
`
`7.70e5
`
`7.65e5
`
`7.60e5
`
`7.55e5
`
`7.50e5
`
`7.45e5
`
`7.40e5
`
`Intensity, cps
`
`200
`
`250
`
`300
`
`350
`
`400
`
`450
`m/z, Da
`
`500
`
`550
`
`600
`
`650
`
`700
`
`Page 27 of 31
`
`

`

` NuMega Resonance Labs
` Sample Name: 13-113-2X 2007KEYS.731A
` Acq. Date: Thursday, October 22,
` 2020
` -Q1: 12 MCA scans from Sample 28 (13-113-2X 2007KEYS.731A) of 2010KEY...
`
` Polarity/Scan Type: Negative Q1 MS
`
`Max. 2.6e6 cps.
`
`491.0
`
`445.1
`
`409.0
`
`2.5e6
`
`2.4e6
`
`2.3e6
`
`2.2e6
`
`2.1e6
`
`2.0e6
`
`1.9e6
`
`1.8e6
`
`1.7e6
`
`1.6e6
`
`1.5e6
`
`1.4e6
`
`1.3e6
`
`1.2e6
`
`1.1e6
`
`Intensity, cps
`
`1.0e6
`200
`
`250
`
`300
`
`350
`
`400
`
`450
`m/z, Da
`
`500
`
`550
`
`600
`
`650
`
`700
`
`Page 28 of 31
`
`

`

` NuMega Resonance Labs
` Sample Name: 13-115-1X 2007KEYS.731B
` Acq. Date: Thursday, October 22,
` 2020
` +Q1: 12 MCA scans from Sample 32 (13-115-1X 2007KEYS.731B) of 2010KE...
`
` Polarity/Scan Type: Positive Q1 MS
`
`Max. 1.1e6 cps.
`
`411.1
`
`433.0
`450
`m/z, Da
`
`500
`
`550
`
`600
`
`650
`
`700
`
`1.10e6
`1.08e6
`1.06e6
`1.04e6
`1.02e6
`1.00e6
`9.80e5
`9.60e5
`9.40e5
`9.20e5
`9.00e5
`8.80e5
`8.60e5
`8.40e5
`8.20e5
`8.00e5
`7.80e5
`7.60e5
`7.40e5
`7.20e5
`
`Intensity, cps
`
`200
`
`250
`
`300
`
`350
`
`400
`
`Page 29 of 31
`
`

`

` NuMega Resonance Labs
` Sample Name: 13-115-1X 2007KEYS.731B
` Acq. Date: Thursday, October 22,
` 2020
` -Q1: 12 MCA scans from Sample 33 (13-115-1X 2007KEYS.731B) of 2010KEY...
`
` Polarity/Scan Type: Negative Q1 MS
`
`Max. 4.2e6 cps.
`
`444.9
`
`409.0
`
`447.1
`
`250
`
`300
`
`350
`
`400
`
`450
`m/z, Da
`
`500
`
`550
`
`600
`
`650
`
`700
`
`4.2e6
`
`4.0e6
`
`3.8e6
`
`3.6e6
`
`3.4e6
`
`3.2e6
`
`3.0e6
`
`2.8e6
`
`2.6e6
`
`2.4e6
`
`2.2e6
`
`2.0e6
`
`1.8e6
`
`1.6e6
`
`1.4e6
`200
`
`Intensity, cps
`
`Page 30 of 31
`
`

`

`Report #
`
`Company:
`
`Key Synthesis LLC
`
`Address:
`
`‘3
`
`‘ Telephone:
`Name:
`
`1 P0#
`
`804 Primrose Lane
`
`
`Wynntivvood, PA 19296
`
`
`610-362-3281
`Fm:
`
`Ron Bihovsky
`Date:
`
`10/ o D, 6
`
`Email:
`
`rbihovsky@keys
`
`NuMega
`11526 Sorrento Valley Road Ste.B2
`San Diego, CA 92121
`Tel: (858)793-6057 Fax: (858)793-2607
`http://www.Numegalalbsxom
`Numegalab@numegalabs.com
`
`
`ll l,-.’_> l,Cl3 Solvent
`
`Sample II)
`
`NMRT
`MW"-..
`
` Elemental Analysis
`
`
`
`
`Theoretical %
`please continue *
`
`
`
`
`
`* Elemental Analvsi
`_s {3 mg per rug) finglezl
`“ my.WW ._ , Slim?"
`-o.5 to z'» mm, integraww.
`TNMRQDF):
`‘ "(4k picking for H-l, 0-200 ppm, peak picking for C-13. (FID: pleaee request)
`t?i)Cl;(7.26), or D20 (4.78).
`Chemical shifi(H-1). r;
`o), umso <1: ‘
`r*Mass: 1mg in lmL or 20-50 MM , positive H‘Nl negative modes. Please specify MW range.
`
`
`our Instructions /Rm~ :1 [kg (Hygroscopic, Explosive, Volatile, Toxicity,
`
`
`
`JDuplicate: .Or Du ulicate if not in rane: - %
`
`Storage, EA theoretical %, etc.)
`
`
`
`
`
`
`
`amintziins spectral infi, ‘mation in strict confidenc
`
`For NuMega Use Ogly
`
`
`
`: Nqu: 7
`Confidentiali
`
`Comment from Analyst:
`
`Page 31 of31
`l
`
`
`
`Total Charge:
`
`3
`
`Page 31 of 31
`
`

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